Preparation method of an antibacterial tooth growth restoration material

A technology for repairing materials and teeth, which is applied in the preparation of antibacterial tooth growth restoration materials, and in the field of tooth surface growth and restoration antibacterial tooth materials. Small grain size, good bonding, and good structural stability

Active Publication Date: 2018-05-01
福建省诺希科技园发展有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the inventive material does not contain antibacterial elements, so it does not have antibacterial and antibacterial effects. At the same time, the main component of the patented tooth growth restoration material is not hydroxyapatite. There is a certain gap in compatibility with the human body, which may easily cause discomfort to the human body.

Method used

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  • Preparation method of an antibacterial tooth growth restoration material
  • Preparation method of an antibacterial tooth growth restoration material

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Embodiment Construction

[0032] Provide the best embodiment of the present invention below: a kind of preparation method of hydrothermal synthetic antibacterial tooth growth restorative material, adopt the method for natural growth of crystal, prepare antibacterial tooth growth restorative material by hydrothermal synthesis method, at first prepare by water-soluble The binary polyelectrolyte complex composed of cationic polyelectrolyte and organic polybasic acid will contain 40mg / ml polycrotonamide and 24wt% maleic acid in water. Next, copper sulfate, silver nitrate, calcium nitrate tetrahydrate and calcium dihydrogen phosphate were added to the above solution and stirred for 45 minutes. Wherein, the concentration of copper sulfate is 0.05 mol / L, the concentration of silver nitrate is 0.05 mol / L, the concentration of calcium nitrate is 0.14 mol / L, and the molar ratio of calcium / phosphorus (Ca / P) is 1.7. Subsequently, the reaction solution is poured into a hydrothermal kettle, and the above-mentioned t...

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Abstract

The invention belongs to the field of inorganic nonmetal materials, particularly belongs to a preparation method of an anti-bacterial tooth growing and repairing material, and relates to a growing and repairing anti-bacterial tooth material used in an alveolar cavity without a tooth or on the surface of an incomplete tooth. The anti-bacterial tooth growing and repairing material comprises the following main ingredients: apatite crystals containing silver, copper, calcium and phosphorus, titanium oxide and zinc oxide. Under the regulation and control effect of a binary polyelectrolyte compound consisting of water-soluble cationic polyelectrolyte and organic polyatomic acids, ingredients of the tooth growing and repairing material are synthesized with soluble calcium salt, soluble phosphate, copper sulfate and silver nitrate salt, a crystal natural growing method is used, and a dental matrix comprising the apatite crystals containing the silver, the copper, the calcium and the phosphorus, the titanium oxide and the zinc oxide are subjected to adsorption reaction fully. Crystalline grains of the anti-bacterial tooth growing and repairing material are in nanoscale, the copper and the silver can be fine and are uniformly distributed in the tooth growing and repairing material, diameters of metal particles are 30-80 nanometers, and the anti-bacterial tooth growing and repairing material can release anti-bacterial elements quickly and continuously.

Description

technical field [0001] The invention belongs to the field of inorganic non-metallic materials, in particular to a preparation method of an antibacterial tooth growth restoration material, which relates to an antibacterial tooth material for growth and restoration in the alveolar of missing teeth or on the surface of incomplete teeth. The main components are silver, copper, calcium and Apatite crystals of phosphorus, titanium oxide and zinc oxide. Background technique [0002] At present, the demand for dental oral materials is increasing year by year. Among them, dental oral materials such as titanium alloy and nickel-chromium alloy are in great demand in life. With the improvement of people's living standards, artificial tooth materials can maintain the same color as natural teeth. It is very important. Therefore, it is usually necessary to attach a layer of enamel to the surface of titanium alloy and nickel-chromium alloy. The enamel layer is the white translucent hard tis...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A61K6/033A61K6/027A61K6/838
Inventor 郑祖辉徐淑波
Owner 福建省诺希科技园发展有限公司
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