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35results about How to "Improve room temperature toughness" patented technology

High-strength Mg-Gd-Y-Zn-Mn alloy

The present invention relates to a high-strength Mg-Gd-Y-Zn-Mn alloy. The alloy comprises the following alloying elements distributed in the alloy, by weight, 8.2-10.2% of Gd, 5.0-6.0% of Y, 0.5-4.0% of Zn, 0.5-0.8% of Mn, and the balance of Mg and inevitable impurities. The alloy is prepared by adopting the following process: material preparing, vacuum melting and ingot casting, uniformization annealing, extrusion and heat treatment. According to the present invention, Mg, Zn, Gd and Y form a large amount of long period phases in the Mg-Gd-Y-Zn-Mn alloy so as to provide a significant dispersion strengthening effect, and the time effect treatment is adopted to introduce the strengthening effect of the metastable phase; the process is a preparation method for the high-strength deformation Mg alloy, wherein the method integrates solid solution strengthening, precipitation strengthening and deformation strengthening; the method has characteristics of simple process, strong portability, easy operation and low cost; with the method, tensile strength and yield strength of the allay at the room temperature are significantly improved, and difficulty of allay application limitation due to low mechanical property is solved so as to expand the application range of the Mg alloy.
Owner:重庆昱华新材料科技有限公司

Method for manufacturing nanometer antibacterial ceramic glaze layers

InactiveCN105152683ASpectrum antimicrobialQuick releaseArgon atmosphereMetallic materials
The invention belongs to the field of inorganic nonmetal materials, particularly discloses a method for manufacturing nanometer antibacterial ceramic glaze layers, and relates to methods for manufacturing ceramic glaze layers. Antibacterial elements are added into ceramic glaze layer bases to carry out antibacterial disinfection on the ceramic glaze layers. Precursors for superfine powder of the nanometer antibacterial ceramic glaze layers comprise 45-60% of SiO<2>, 10-14%of Al<2>O<3>, 7-10% of CaO, 5-7% of ZnO, 2-5% of CuO, 3-6% of MgO, 1-3% of TiO<2> and 0.2-2% of Ag<2>O. The method includes filling graphite containers with the precursors for proportionally preparing the superfine powder of the nanometer antibacterial ceramic glaze layers; preserving heat for 120min-240min under argon atmosphere protection and the condition of temperatures of 1250-1400 DEG C to carry out synthesis; adding absolute ethyl alcohol into a ball-mill to carry out mechanical ball-milling for 24 hours so as to obtain the superfine precursor powder with crystal grain sizes of 30-80nm. The method has the advantages that metal grains of zinc, copper, magnesium and silver are fine and are uniformly distributed in glaze layers, the diameters of the metal grains are 30-80nm, and antibacterial elements can be quickly, durably and continuously released.
Owner:SHANDONG JIANZHU UNIV

High-toughness cold-hot-fatigue-resistant cast steel for high-speed train brake disc and preparation method thereof

ActiveCN111360198AMatch mechanicsMatching cold and heat fatigue resistanceFoundry mouldsFurnace typesBrakeMetallic materials
The invention relates to high-toughness cold-hot-fatigue-resistant cast steel for a high-speed train brake disc and a preparation method thereof, belongs to the field of metal materials and preparation thereof, and solves the problem of matching of room-temperature toughness, high-temperature mechanical properties and cold and hot fatigue failure resistance of the cast steel for the high-speed train brake disc in the prior art. The high-toughness cold-hot-fatigue-resistant cast steel for the high-speed train brake disc comprises the following chemical components, in percentage by mass, of 0.20%-0.40% of C, 0.30%-0.70% of Si, 0.50%-2.00% of Mn, 0.50%-2.00% of Cr, 0.50%-2.00% of Ni, 0.40%-1.80% of Mo, 0.01%-0.30% of V, smaller than or equal to 0.015% of P, smaller than or equal to 0.010% ofS, smaller than or equal to 0.010% of O, smaller than or equal to 0.015% of N, and the balance Fe and inevitable impurities, wherein the total content of the Mn, the Cr and the Ni is 2.00%-6.00%, andthe total content of the Mo and the V is 0.41%-2.00%. Through reasonable composition, organization structure and preparation process regulation and control, excellent room-temperature toughness, high-temperature mechanical property and cold and hot fatigue failure resistance of the cast steel are matched, the requirements for comprehensive mechanical property and long service life of the cast steel brake disc of a high-speed train are met, and the cast steel is suitable for being used as a material for the cast steel brake disc of the high-speed train.
Owner:ADVANCED MFG TECH CENT CHINA ACAD OF MASCH SCI & TECH +1

Preparation method enabling super-plastic magnesium alloy to have approximately-spherical precipitated phase

The invention discloses a preparation method enabling a super-plastic magnesium alloy to have an approximately-spherical precipitated phase. The preparation method enabling the super-plastic magnesium alloy to have the approximately-spherical precipitated phase comprises three steps of homogenizing treatment, temperature-variable rolling grain refining and precipitated phase rounding adjustment. According to the preparation method enabling the super-plastic magnesium alloy to have the approximately-spherical precipitated phase, firstly, a magnesium alloy oversaturated solid solution is prepared through high-temperature and low-temperature staged heat treatment; secondly, dynamic recrystallization is induced through high-temperature large-reduction-rate medium-and-low-speed rolling, twin crystal refining is induced through low-temperature small-reduction-rate rapid rolling, and recrystallized grains are hindered from growing at low temperature; and the rounding heat treatment parameter is further adjusted, and a wrought magnesium alloy structure which is provided with submicron and micron matrix grains and has the approximately-spherical randomly-distributed precipitated phase is prepared. The preparation method enabling the super-plastic magnesium alloy to have the approximately-spherical precipitated phase can significantly improve the indoor-temperature strength and toughness of the magnesium alloy and is beneficial for full play of high-temperature superplasticity potential of the magnesium alloy. The preparation method enabling the super-plastic magnesium alloy to have the approximately-spherical precipitated phase breaks through the technical constraint that a traditional rolled structure cannot reach superplasticity, is particularly suitable for rolling of the magnesium alloy containing two or more kinds of high-volume-fraction mixed precipitated phases and improves the rolling efficiency.
Owner:JILIN UNIV

High-temperature-resistant multi-component silicide coating on surface of niobium alloy and preparation method of high-temperature-resistant multi-component silicide coating

ActiveCN109023338AInhibition of medium temperature "pest" oxidationImprove high temperature oxidation resistanceHeat inorganic powder coatingNiobium alloyMetal powder
The invention discloses a high-temperature-resistant multi-component silicide coating on the surface of niobium alloy and a preparation method of the high-temperature-resistant multi-component silicide coating. The high-temperature-resistant multi-component silicide coating has the phase composition of [(Nb(1-x-y)TixCry)(1-z),Rz]Si2, wherein R is one or more of the metal elements of Mo, W, Zr, Hfand Ta; x, y and z respectively represent mole numbers of the corresponding elements; 0.05<=x<=0.2; 0.05<=y<=0.3; and 0.05<=z<=0.4. The preparation method comprises the following steps: first, metal elementary powder and silicon elementary powder are weighed and thrown into a mixer to be fully mixed for 12-24 h; the mixed multi-component metal powder covers a niobium alloy workpiece, then, the covered niobium alloy workpiece is placed in a graphite crucible, and the graphite crucible is placed in a discharge plasma sintering furnace for sintering; and a sample of the sintered coating is subjected to homogenization heat treatment in a vacuum or protective atmosphere. The invention provides the discharge plasma sintering and homogenization heat treatment compounded preparation process. The process is simple. The coating structure is homogeneous. Ingredients are controllable. The coating has favorable high-temperature oxidation resistance at 1,200-1,600 DEG C.
Owner:CHINA UNIV OF MINING & TECH

Hydrothermal synthesis method for preparation of nano antibacterial tooth enamel layer

The invention belongs to the field of inorganic nonmetallic materials, particularly discloses a hydrothermal synthesis method for preparation of a nano antibacterial tooth enamel layer and relates to attachment of the antibacterial tooth enamel layer in a general thickness of 0.2-0.8mm onto the surface of an artificial tooth, wherein the antibacterial tooth enamel layer is mainly made from apatite crystals containing silver, copper, calcium and phosphate. Under the control of a dual-polyelectrolyte compound consisting of water-soluble cation polyelectrolyte and organic polyatomic acid, the artificial tooth is put into soluble calcium salts, soluble phosphates, copper sulfate and silver nitrate salts to realize synthesis to finally cover the artificial tooth with the antibacterial tooth enamel layer in the general thickness of 0.2-0.8mm. The antibacterial tooth enamel layer is mainly made from apatite crystals containing silver, copper, calcium and phosphate, and crystal grains of the enamel layer are nanoscale crystal grains, so that copper and silver metallic particles smaller in size can be distributed in the enamel more uniformly; the metallic particles are 30-80nm in diameter, and antibacterial elements can be released quickly and constantly.
Owner:福建省诺希科技园发展有限公司 +1

Method for preparing hydroxyapatite film layer on magnesium alloy surface

The invention discloses a method for preparing a hydroxyapatite film layer on a magnesium alloy surface, and is applicable to surface processing of medical magnesium alloy. Soluble calcium salt and soluble phosphate are adopted for performing surface processing on the medical magnesium alloy to obtain a layer of film with the main content of a hydroxyapatite crystal containing calcium and phosphorus, so that the human body compatibility of the medical magnesium alloy is improved. According to the method, a unit doublet polyelectrolyte complex solution consisting of a water soluble cation polyelectrolyte and and an organic polyatomic acid is prepared, and the solution is prepared from a water solution containing polybutylamide with the concentration of 40 mg / ml and 24wt% of maleic acid. Then calcium nitrate terahydrate and monocalcium phosphate are added into the solution, and the solution is stirred for 45 minutes, wherein the concentration of calcium nitrate is 0.14 mol / L, and the molar ratio of calcium to phosphorus is 1.7. The medical magnesium alloy is added into a hydrothermal kettle and is reacted for 100 hours at a temperature of 90 DEG C, so that the nano-antibacterial hydroxyapatite film layer and the medical magnesium alloy are subjected to full adsorption reaction, and a layer of hydroxyapatite crystal film is formed on the surface of the medical magnesium alloy.
Owner:SHANDONG JIANZHU UNIV

Preparing method of high-strength copper-based composite toughened by boron carbide and silicon carbide crystal whiskers

The invention belongs to the field of nonferrous metal composites, in particular to a method for toughening a high-strength copper-based composite by nanometer boron carbide and silicon carbide crystal whiskers. An in-situ generated high-strength copper-based composite powder toughened by boron carbide and silicon carbide crystal whiskers consists of high-strength copper-based composite base material powder and nanometer boron carbide and silicon carbide crystal whisker powder. The high-strength copper-based composite base powder is uniformly mixed with the nanometer boron carbide and silicon carbide crystal whisker powder by a mechanical mixing process, a vacuum-sintered hot-pressed ingot is enabled to deform through extrusion, and the in-situ generated high-strength copper-based composite toughened by the nanometer boron carbide and silicon carbide crystal whiskers is obtained. As the in-situ generated copper-based composite toughened by the nanometer boron carbide and silicon carbide crystal whiskers has high tenacity, and at the same time, the wear resistance and the strength are greatly improved, the copper-based composite is particularly suitable for high-speed railway high-strength cables, high-end equipment manufacturing industry and the like and is particularly suitable for being used as a material for cutters, dies, aviation, aerospace and the like.
Owner:SHANDONG JIANZHU UNIV

High-toughness, heat-resistant and cold-fatigue-resistant high-speed train brake disc cast steel and preparation method thereof

ActiveCN111360198BImproved resistance to cold and heat fatigueInhibition of germinationFoundry mouldsFurnace typesThermal fatigueBrake
The invention relates to a cast steel for high-speed train brake discs with high toughness and anti-cold and heat fatigue and a preparation method thereof, which belongs to the field of metal materials and their preparation, and solves the problem of room temperature strength, toughness and high temperature of cast steel for high-speed train brake discs in the prior art. Matching of mechanical properties and thermal fatigue resistance failure performance. A high-toughness and heat-resistant fatigue-resistant cast steel for high-speed train brake discs, the chemical composition of which is: C: 0.20%-0.40%, Si: 0.30%-0.70%, Mn: 0.50%-2.00%, Cr : 0.50%‑2.00%, Ni: 0.50%‑2.00%, Mo: 0.40%‑1.80%, V: 0.01%‑0.30%, P≤0.015%, S≤0.010%, O≤0.010%, N≤0.015% , the rest are Fe and unavoidable impurities; the total content of Mn+Cr+Ni is 2.00%-6.00%, and the total content of Mo+V is 0.41%-2.00%. Through reasonable composition, organizational structure and preparation process control, the combination of excellent room temperature strength and toughness, high temperature mechanical properties and cold and heat fatigue resistance failure performance of cast steel is realized, which meets the comprehensive mechanical properties and long service life requirements of high-speed train cast steel brake discs , suitable for high-speed train cast steel brake disc materials.
Owner:BEIJING NAT INNOVATION INST OF LIGHTWEIGHT LTD +1

A high temperature resistant multi-component silicide coating on the surface of niobium alloy and its preparation method

ActiveCN109023338BInhibition of medium temperature "pest" oxidationImprove high temperature oxidation resistanceHeat inorganic powder coatingNiobium alloyMetal powder
The invention discloses a high-temperature-resistant multi-component silicide coating on the surface of niobium alloy and a preparation method of the high-temperature-resistant multi-component silicide coating. The high-temperature-resistant multi-component silicide coating has the phase composition of [(Nb(1-x-y)TixCry)(1-z),Rz]Si2, wherein R is one or more of the metal elements of Mo, W, Zr, Hfand Ta; x, y and z respectively represent mole numbers of the corresponding elements; 0.05<=x<=0.2; 0.05<=y<=0.3; and 0.05<=z<=0.4. The preparation method comprises the following steps: first, metal elementary powder and silicon elementary powder are weighed and thrown into a mixer to be fully mixed for 12-24 h; the mixed multi-component metal powder covers a niobium alloy workpiece, then, the covered niobium alloy workpiece is placed in a graphite crucible, and the graphite crucible is placed in a discharge plasma sintering furnace for sintering; and a sample of the sintered coating is subjected to homogenization heat treatment in a vacuum or protective atmosphere. The invention provides the discharge plasma sintering and homogenization heat treatment compounded preparation process. The process is simple. The coating structure is homogeneous. Ingredients are controllable. The coating has favorable high-temperature oxidation resistance at 1,200-1,600 DEG C.
Owner:CHINA UNIV OF MINING & TECH

Method for manufacturing non-oriented high-silicon steel cold-rolled sheet based on strip casting and did

ActiveCN105063473BOptimization of "strain-induced disorder" effectDecreased macrohardnessReduction rateRoom temperature
The invention relates to a method for manufacturing a non-oriented high-silicon steel cold-rolled sheet based on strip cast rolling and DID (deformation induced disordering), belonging to the technical field of metallurgy. The method comprises the following steps: (1) smelting liquid steel, wherein the liquid steel comprises the following components in percentage by weight: less than or equal to 0.005% of C, 6.4%-6.6% of Si, less than or equal to 0.003% of N, less than or equal to 0.003% of O, less than or equal to 0.005% of S and the balance of Fe; (2) carrying out cast rolling by virtue of sheet cast rolling equipment, and carrying out air cooling until reaching the room temperature; (3) manufacturing hot rolled plates by virtue of hot rolling; (4) manufacturing warm rolled plates by virtue of warm rolling, wherein a strain induced disorder effect is generated during the warm rolling; (5) manufacturing cold rolled plates by virtue of cold rolling; and (6) carrying out annealing at 900-1150 DEG C. According to the method, by virtue of a strip cast rolling process, the optimal warm-rolling reduction rate is selected, and an intermediate annealing process is omitted, so that the energy consumption is reduced, the magnetic performance of products after annealing is excellent, the procedures are simple, and equipment requirements are low.
Owner:NORTHEASTERN UNIV LIAONING

Preparation method of boron carbide-silicon carbide whisker toughened high-strength copper matrix composite

The invention belongs to the field of nonferrous metal composites, in particular to a method for toughening a high-strength copper-based composite by nanometer boron carbide and silicon carbide crystal whiskers. An in-situ generated high-strength copper-based composite powder toughened by boron carbide and silicon carbide crystal whiskers consists of high-strength copper-based composite base material powder and nanometer boron carbide and silicon carbide crystal whisker powder. The high-strength copper-based composite base powder is uniformly mixed with the nanometer boron carbide and silicon carbide crystal whisker powder by a mechanical mixing process, a vacuum-sintered hot-pressed ingot is enabled to deform through extrusion, and the in-situ generated high-strength copper-based composite toughened by the nanometer boron carbide and silicon carbide crystal whiskers is obtained. As the in-situ generated copper-based composite toughened by the nanometer boron carbide and silicon carbide crystal whiskers has high tenacity, and at the same time, the wear resistance and the strength are greatly improved, the copper-based composite is particularly suitable for high-speed railway high-strength cables, high-end equipment manufacturing industry and the like and is particularly suitable for being used as a material for cutters, dies, aviation, aerospace and the like.
Owner:SHANDONG JIANZHU UNIV

A preparation method for synthesizing nano antibacterial tooth enamel layer by hydrothermal method

The invention belongs to the field of inorganic nonmetallic materials, particularly discloses a hydrothermal synthesis method for preparation of a nano antibacterial tooth enamel layer and relates to attachment of the antibacterial tooth enamel layer in a general thickness of 0.2-0.8mm onto the surface of an artificial tooth, wherein the antibacterial tooth enamel layer is mainly made from apatite crystals containing silver, copper, calcium and phosphate. Under the control of a dual-polyelectrolyte compound consisting of water-soluble cation polyelectrolyte and organic polyatomic acid, the artificial tooth is put into soluble calcium salts, soluble phosphates, copper sulfate and silver nitrate salts to realize synthesis to finally cover the artificial tooth with the antibacterial tooth enamel layer in the general thickness of 0.2-0.8mm. The antibacterial tooth enamel layer is mainly made from apatite crystals containing silver, copper, calcium and phosphate, and crystal grains of the enamel layer are nanoscale crystal grains, so that copper and silver metallic particles smaller in size can be distributed in the enamel more uniformly; the metallic particles are 30-80nm in diameter, and antibacterial elements can be released quickly and constantly.
Owner:福建省诺希科技园发展有限公司 +1

Preparation method of an antibacterial tooth growth restoration material

The invention belongs to the field of inorganic nonmetal materials, particularly belongs to a preparation method of an anti-bacterial tooth growing and repairing material, and relates to a growing and repairing anti-bacterial tooth material used in an alveolar cavity without a tooth or on the surface of an incomplete tooth. The anti-bacterial tooth growing and repairing material comprises the following main ingredients: apatite crystals containing silver, copper, calcium and phosphorus, titanium oxide and zinc oxide. Under the regulation and control effect of a binary polyelectrolyte compound consisting of water-soluble cationic polyelectrolyte and organic polyatomic acids, ingredients of the tooth growing and repairing material are synthesized with soluble calcium salt, soluble phosphate, copper sulfate and silver nitrate salt, a crystal natural growing method is used, and a dental matrix comprising the apatite crystals containing the silver, the copper, the calcium and the phosphorus, the titanium oxide and the zinc oxide are subjected to adsorption reaction fully. Crystalline grains of the anti-bacterial tooth growing and repairing material are in nanoscale, the copper and the silver can be fine and are uniformly distributed in the tooth growing and repairing material, diameters of metal particles are 30-80 nanometers, and the anti-bacterial tooth growing and repairing material can release anti-bacterial elements quickly and continuously.
Owner:福建省诺希科技园发展有限公司
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