Hydrothermal synthesis method for preparation of nano antibacterial tooth enamel layer
A technology of enamel layer and hydrothermal method, used in dental preparations, dentistry, dental prostheses, etc., can solve the problems of non-sterilization and antibacterial, and achieve the effects of good tissue stability, improved wear resistance and hardness, and uniform distribution.
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[0030] Provide the best embodiment of the present invention below: a kind of preparation method of nano antibacterial tooth enamel layer synthesized by hydrothermal method, adopt the method for crystal natural growth, generate nano antibacterial tooth enamel layer material on artificial denture surface by hydrothermal synthesis method, Firstly, a binary polyelectrolyte complex composed of water-soluble cationic polyelectrolyte and organic polybasic acid is prepared, which will contain an aqueous solution of 40mg / ml polycrotonamide and 24wt% urea. Next, copper sulfate, silver nitrate, calcium nitrate tetrahydrate and calcium dihydrogen phosphate were added to the above solution and stirred for 45 minutes. Wherein, wherein the concentration of copper sulfate is 0.05mol / L, the concentration of silver nitrate is 0.05mol / L, the concentration of calcium nitrate is 0.14mol / L, and the molar ratio of calcium / phosphorus (Ca / P) is 1.7. Then pour the reaction solution into a hydrothermal ...
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