Hydrothermal synthesis method for preparation of nano antibacterial tooth enamel layer

A technology of enamel layer and hydrothermal method, used in dental preparations, dentistry, dental prostheses, etc., can solve the problems of non-sterilization and antibacterial, and achieve the effects of good tissue stability, improved wear resistance and hardness, and uniform distribution.

Active Publication Date: 2015-12-16
福建省诺希科技园发展有限公司 +1
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Problems solved by technology

However, this invention material does not contain antibacterial elements, and it does not have antibacterial and antibacterial effects. Other antibacterial patents such as tooth enamel coating liquid and fluoride toothpaste can only play a short-term antibacterial and antibacterial effect. It is very necessary to add antibacterial elements to the enamel layer matrix for antibacterial and anti-virus preparation methods

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  • Hydrothermal synthesis method for preparation of nano antibacterial tooth enamel layer
  • Hydrothermal synthesis method for preparation of nano antibacterial tooth enamel layer

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Embodiment Construction

[0030] Provide the best embodiment of the present invention below: a kind of preparation method of nano antibacterial tooth enamel layer synthesized by hydrothermal method, adopt the method for crystal natural growth, generate nano antibacterial tooth enamel layer material on artificial denture surface by hydrothermal synthesis method, Firstly, a binary polyelectrolyte complex composed of water-soluble cationic polyelectrolyte and organic polybasic acid is prepared, which will contain an aqueous solution of 40mg / ml polycrotonamide and 24wt% urea. Next, copper sulfate, silver nitrate, calcium nitrate tetrahydrate and calcium dihydrogen phosphate were added to the above solution and stirred for 45 minutes. Wherein, wherein the concentration of copper sulfate is 0.05mol / L, the concentration of silver nitrate is 0.05mol / L, the concentration of calcium nitrate is 0.14mol / L, and the molar ratio of calcium / phosphorus (Ca / P) is 1.7. Then pour the reaction solution into a hydrothermal ...

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Abstract

The invention belongs to the field of inorganic nonmetallic materials, particularly discloses a hydrothermal synthesis method for preparation of a nano antibacterial tooth enamel layer and relates to attachment of the antibacterial tooth enamel layer in a general thickness of 0.2-0.8mm onto the surface of an artificial tooth, wherein the antibacterial tooth enamel layer is mainly made from apatite crystals containing silver, copper, calcium and phosphate. Under the control of a dual-polyelectrolyte compound consisting of water-soluble cation polyelectrolyte and organic polyatomic acid, the artificial tooth is put into soluble calcium salts, soluble phosphates, copper sulfate and silver nitrate salts to realize synthesis to finally cover the artificial tooth with the antibacterial tooth enamel layer in the general thickness of 0.2-0.8mm. The antibacterial tooth enamel layer is mainly made from apatite crystals containing silver, copper, calcium and phosphate, and crystal grains of the enamel layer are nanoscale crystal grains, so that copper and silver metallic particles smaller in size can be distributed in the enamel more uniformly; the metallic particles are 30-80nm in diameter, and antibacterial elements can be released quickly and constantly.

Description

technical field [0001] The invention belongs to the field of inorganic non-metallic materials, in particular to a method for preparing a nanometer antibacterial tooth enamel layer, which involves attaching a layer of antibacterial tooth enamel layer with a thickness of usually 0.2-0.8mm on the surface of artificial teeth, the main components of which are silver, copper, Apatite crystals of calcium and phosphorus. Background technique [0002] At present, the demand for dental oral materials is increasing year by year. Among them, dental oral materials such as titanium alloy and nickel-chromium alloy are in great demand in life. With the improvement of people's living standards, artificial tooth materials can maintain the same color as natural teeth. It is very important. Therefore, a layer of enamel is usually attached to the surface of titanium alloy and nickel-chromium alloy. The enamel layer is a white translucent hard tissue with the highest degree of calcification cover...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A61K6/033A61K6/04A61K6/838
Inventor 徐淑波李振东张晓东任国成刘婷
Owner 福建省诺希科技园发展有限公司
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