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Preparation method of highly stable cellulose-based natural edible anthocyanin pigment complex

A cellulose-based, high-stability technology, applied in the field of preparation of natural food pigments, can solve the problems of restricting extensive development and application, improving the stability of pigments, and hidden health hazards, so as to reduce the harm to human health and effectively Absorption and utilization, the effect of simple preparation process

Active Publication Date: 2018-08-17
ZHEJIANG JINCHANG SPECIALTY PAPER CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0017] Disadvantages: 1. There is still a lot of room for improvement in the duration of action of its composite pigments
2. The effective dispersion and stability of water-insoluble pigments in water-based systems are still poor
[0018] In the above invention patents 1-5, there is no mention of using the colloidal particles of cellulose substances and their derivatives as the carrier of natural food pigments to improve the stability of the pigments and prolong their duration of action; in addition, this patent also Does not take into account the transformation of the complex pigment solvent system
[0019] In addition, in the prior art, the preparation results surrounding pigment complex emulsions show that when water-insoluble pigments are used as raw materials, it is difficult to prepare water-based pigment complexes, and the use of a large amount of organic solvents causes hidden Issues such as sexual health hazards and environmental pollution have become an important reason restricting its extensive development and application
At the same time, whether it is water-soluble or water-insoluble natural pigment preparations, their poor stability and short effective period have also made them suffer from criticism.

Method used

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  • Preparation method of highly stable cellulose-based natural edible anthocyanin pigment complex
  • Preparation method of highly stable cellulose-based natural edible anthocyanin pigment complex

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0066] A method for preparing a high-stability cellulose-based natural edible anthocyanin pigment compound. The cellulose-based natural edible anthocyanin pigment compound is refined from a two-part composition of a main material and an auxiliary material. The main material includes The functional ingredient anthocyanin and the colloidal solution of cellulose substances or their derivatives with a size of nano / micron scale obtained by degrading natural fibers loaded with functional ingredients, and the auxiliary materials include stabilizers and polysaccharide thickeners, so The cellulose-based natural edible anthocyanin pigment complex is a water-based cellulose-based natural edible anthocyanin pigment complex emulsion, and the water-based cellulose-based natural edible anthocyanin pigment complex emulsion undergoes post-processing to obtain A cellulose-based natural edible anthocyanin pigment compound granule is prepared, and its preparation method includes 1 material prepara...

Embodiment 2

[0101] A method for preparing a high-stability cellulose-based natural edible anthocyanin pigment compound. The preparation process steps are the same as in Example 1 (solid particles), except that the main ingredient used is water-soluble / alcohol-soluble sorghum The base material of the red pigment and the loaded functional component is cellulose microfiber (MFC), and no thickener is added to the base mother liquor, and its preparation method includes 1 material preparation and 2 preparation process:

[0102] 1 preparation

[0103] 1-1 main material

[0104] 1-1-1 Functional ingredient: Anthocyanin, in this embodiment, sorghum red pigment is selected.

[0105] 1-1-2 Substrate: colloidal solution of nano / micro cellulose substances or derivatives thereof, in this embodiment, cellulose microfiber (MFC) is selected;

[0106] 1-2 accessories

[0107] 1-2-1 stabilizer: the present embodiment still selects malic acid;

[0108] 1-2-2 Polysaccharide thickener: no thickener is adde...

Embodiment 3

[0122] A method for preparing a high-stability cellulose-based natural edible anthocyanin pigment compound, the preparation method comprising 1 material preparation and 2 preparation processes:

[0123] 1 preparation

[0124] 1-1 main material

[0125] 1-1-1 functional component: anthocyanin (Anthocyanin), in the present embodiment, select mulberry red pigment for use;

[0126] 1-1-2 Substrate: colloidal solution of nano / micro cellulose substances or derivatives thereof, in this embodiment, carboxy cellulose nanocrystals (CNCC) are selected;

[0127] 1-2 accessories

[0128] 1-2-1 stabilizer: the present embodiment selects tea polyphenols of polyphenols;

[0129] 1-2-2 polysaccharide thickener: Lycium barbarum polysaccharide is selected for use in this embodiment;

[0130] 2 Preparation process

[0131] 2-1 formula

[0132] Preparation of material formula for solid particle composite product

[0133] components

Amount (mass fraction, based on the total weig...

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Abstract

The invention discloses a preparation method of a high-stability cellulose base natural edible anthocyan pigment compound. The compound consists of two parts of main materials and auxiliary materials, wherein the main materials comprise anthocyan as a functional component, and a nanometer / micron cellulose substance or a derivative colloidal solution thereof as a base material, wherein the nanometer / micron cellulose substance or the derivative colloidal solution thereof is used for loading the functional component; the auxiliary materials contain a stabilizing agent and a polysaccharide thickening agent. The preparation method comprises the following steps: at a lower rotating speed, dropwise adding an aqueous / organic solvent solution of anthocyan natural pigment into a pre-sheared base material mother solution using a cellulose base colloidal solution as a main component, and shearing the aqueous / organic solvent solution of the anthocyan natural pigment at a high speed so as to obtain the cellulose base pigment compound. The pigment compound is an aqueous-based anthocyan pigment compound emulsion which is post-processed and treated to be prepared into solid granules of the anthocyan pigment compound, the anthocyan pigment compounds of various forms can be well dispersed in water, the storage stability of the pigment can be improved, and the action period of the pigment can be prolonged.

Description

technical field [0001] The invention relates to a preparation method of a natural food coloring compound with good stability, in particular to a preparation method of a highly stable cellulose-based natural food anthocyanin coloring compound, which belongs to the technical field of preparation of natural food coloring. Background technique [0002] Natural pigments of plant-derived pigments, microbial pigments and mineral pigments extracted from plants, animals and minerals, among which edible natural pigments are collectively referred to as natural food pigments. In order to improve the color of food or maintain the original color of food, natural food coloring is usually added for coloring during processing. Therefore, natural food coloring is a very important food additive. [0003] Since the chemical structure of natural food coloring mostly contains unsaturated double bonds and other oxidizable groups, it will be oxidized under the action of oxygen in the air, which wil...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A23L5/43
CPCA23V2002/00A23V2200/242A23V2200/00A23V2250/044A23V2250/0616A23V2250/02A23V2250/2104A23V2250/21164A23V2250/2117A23V2250/2132A23V2250/28A23V2250/51A23V2250/5108A23V2250/51084A23V2250/51088
Inventor 孙波张民司传领刘锐吴涛倪永浩
Owner ZHEJIANG JINCHANG SPECIALTY PAPER CO LTD
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