A wave-absorbing honeycomb and its preparation method
A technology of honeycomb and glue, which is applied in the direction of inorganic compound addition, textile and paper making, and fiber raw material processing. It can solve the problems of narrow absorption frequency, inability to meet the needs of wave-absorbing materials, and high density, and achieve the effect of improving wave-absorbing performance.
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Embodiment 1
[0024] A preparation method of absorbing honeycomb:
[0025] 1) Preparation of graphene oxide: Take 100 parts of expanded graphite with a size of 50-300 mesh, add 200 parts of sodium chloride and grind for 30 minutes, then wash with deionized water to remove sodium chloride; add 1000 parts of deionized water, and stir ultrasonically 30min, the ultrasonic power is 700W, then add 300 parts of benzoyl peroxide to it, seal the container and ultrasonic for 2 hours, filter once with filter paper with larger pores, discard the filter residue, choose fine-pore filter paper or centrifuge to obtain the filtrate Graphene oxide spare.
[0026] 2) Preparation of wave-absorbing glue:
[0027] Solution A preparation: Dissolve 1 part of graphene oxide in 50 parts of ethanol-water mixed solvent, and mix uniformly to obtain A solution; wherein the parts by weight of ethanol in the ethanol aqueous solution are 40 parts;
[0028] Preparation of solution B: Dissolve 15 parts of phenolic resin an...
Embodiment 2
[0039] A preparation method of absorbing honeycomb:
[0040] 1) Preparation of graphene oxide: Take 100 parts of expanded graphite with a size of 50-300 mesh, add 200 parts of sodium chloride and grind for 30 minutes, then wash away potassium chloride with deionized water; add 1000 parts of deionized water, and stir ultrasonically 30min, the ultrasonic power is 700W, then add 300 parts of potassium persulfate to it, seal the container and ultrasonic for 2 hours, filter once with filter paper with larger pores, discard the filter residue, and use fine-pore filter paper or centrifugal separation as the filtrate to obtain graphite oxide Alkene spare.
[0041] 2) Preparation of wave-absorbing glue:
[0042] Solution A preparation: Dissolve 10 parts of graphene oxide in 300 parts of ethyl acetate water mixed solvent, and mix uniformly to obtain A solution; wherein the parts by weight of ethyl acetate in the ethyl acetate aqueous solution is 280 parts;
[0043] Solution B preparat...
Embodiment 3
[0053] A preparation method of absorbing honeycomb:
[0054]1) Preparation of graphene oxide: Take 100 parts of expanded graphite with a size of 50-300 mesh, add 200 parts of sodium chloride and grind for 30 minutes, then wash with deionized water to remove sodium chloride; add 1000 parts of deionized water, and stir ultrasonically 30min, the ultrasonic power is 700W, then add 300 parts of benzoyl peroxide to it, seal the container and ultrasonic for 2 hours, filter once with filter paper with larger pores, discard the filter residue, choose fine-pore filter paper or centrifuge to obtain the filtrate Graphene oxide spare.
[0055] 2) Preparation of wave-absorbing glue:
[0056] Preparation of A solution: Dissolve 5 parts of graphene oxide in 100 parts of n-hexane water mixed solvent, and mix uniformly to obtain A solution; wherein the weight parts of n-hexane in the n-hexane aqueous solution is 80 parts;
[0057] Solution B preparation: dissolve 50 parts of polyurethane resi...
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