Angiogenesis inhibitor polypeptide HS-1 and application thereof
An angiogenesis inhibition, HS-1 technology, applied in the field of bioengineering, can solve the problems of patients' quality of life hazards, unsatisfactory curative effect, damage to normal tissues and organs, etc., achieve high-efficiency tumor targeting ability, inhibit tumor growth process and improve Effect
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[0024] (1) The synthesis of HS-1 peptide comprises the following steps:
[0025] 1) Coupling: first swell Fmoc-ASP-RinkamideMBHAresin (fluorenyl methaneoxycarbonyl-aspartic acid-rink amino resin) 0.33 / 2mmol6.06g in DMF, 10ml / g resin, then use 20%piperdine / DMF The solution removes the Fmoc protecting group (hereinafter referred to as decapping), washes the resin after decapping with DMF, adds raw material Fmoc-Arg(tBU)-OH2.3g, and uses HBTU1.44g as the condensing agent. The reaction time is 30 minutes, and the Kaiser method detects , if the test result is negative, it means that the coupling reaction is complete, then proceed to uncap for 30 minutes, if the test result is still positive, it means that the coupling reaction is not completed or the reaction is incomplete, and it is necessary to extend the coupling time or re-feed Coupling until the coupling reaction is complete.
[0026] Repeat the above operation, and sequentially couple Fmoc-Gly(OtBU)-OH,...FmocGly--OH; Fmoc-P...
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