A kind of aldehyde absorption emulsion and preparation method thereof
A technology of emulsion and emulsifier, applied in the field of emulsion, can solve the problem of inability to remove formaldehyde, and achieve the effect of enhancing ability and reducing environmental harm
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Embodiment 1
[0032] The preparation method of absorbing aldehyde emulsion, comprises the steps:
[0033] 1) Mix 15% methyl methacrylate, 11.5% styrene, 20% n-butyl acrylate, 1% functional monomer and 2% emulsifier for pre-emulsification to obtain pre-emulsified monomer;
[0034] 2) Put 50% of water and 0.08% of emulsifier into the reaction kettle, stir, and after heating up to 82-85°C, add 0.21% of initiator and 5% of pre-emulsified monomer to carry out seed polymerization, and react for 10 -12min; raise the temperature to 84-87°C, add 0.09% initiator and the remaining pre-emulsified monomer dropwise to the reaction system, the dropping time is 3.5-4.0h, and keep warm for 1.5-2.0h after the dropping is completed ; Add 0.12% initiator to the reaction system to eliminate residual monomers and keep the temperature for 60-90min.
Embodiment 2
[0036] The preparation method of absorbing aldehyde emulsion, comprises the steps:
[0037] 1) Mix 15% methyl methacrylate, 11% styrene, 20% n-butyl acrylate, 1.5% functional monomer and 2% emulsifier for pre-emulsification to obtain pre-emulsified monomer;
[0038] 2) Put 50% water and 0.08% emulsifier into the reaction kettle, stir, and after heating up to 82-85°C, add 0.21% initiator and 3% pre-emulsified monomer to carry out seed polymerization, and react for 10 -12min; raise the temperature to 84-87°C, add 0.09% initiator and the remaining pre-emulsified monomer dropwise to the reaction system, the dropping time is 3.5-4.0h, and keep warm for 1.5-2.0h after the dropping is completed ; Add 0.12% initiator to the reaction system to eliminate residual monomers and keep the temperature for 60-90min.
Embodiment 3
[0040] The preparation method of absorbing aldehyde emulsion, comprises the steps:
[0041] 1) Mix 15% methyl methacrylate, 10.5% styrene, 20% n-butyl acrylate, 2% functional monomer and 2% emulsifier for pre-emulsification to obtain pre-emulsified monomer;
[0042] 2) Put 50% water and 0.08% emulsifier into the reaction kettle, stir, and after heating up to 82-85°C, add 0.21% initiator and 8% pre-emulsified monomer to carry out seed polymerization, and react for 10 -12min; raise the temperature to 84-87°C, add 0.09% initiator and the remaining pre-emulsified monomer dropwise to the reaction system, the dropping time is 3.5-4.0h, and keep warm for 1.5-2.0h after the dropping is completed ; Add 0.12% initiator to the reaction system to eliminate residual monomers and keep the temperature for 60-90min.
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