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99results about How to "No reflux" patented technology

Hyperbranched hydroxyl polyester resin, and preparation method and application of hyperbranched hydroxyl polyester resin

The invention discloses hyperbranched hydroxyl polyester resin, and a preparation method and an application of the hyperbranched hydroxyl polyester resin.The preparation method of the hyperbranched hydroxyl polyester resin comprises the following steps: 1) according to molar fraction, 1 part of dicarboxylic anhydride and 2-4 parts of polyhydric alcohol are mixed in a reaction kettle, paratoluenesulfonic acid and an organic solvent are added for reaction at 105-125 degrees under nitrogen protection, then 4-10 parts of phthalic anhydride are added, and reaction for 2-3h is carried out; and 2) according to molar fraction, 6-10 parts of epoxy compounds are added to a matrix prepared in the step 1), a catalyst and an organic solvent are added for reaction for 4-6h at 105-1130 degrees under the nitrogen protection till an acid value is less than 10mgKOH / g, and cooling and discharging are carried out. The solid content of the hyperbranched hydroxyl polyester resin reaches above 70%, and the viscosity is 3000-12000mPa.s. High solid-content bi-component polyurethane dope prepared with the adoption of the hyperbranched hydroxyl polyester resin has high construction solid content, low VOC content, high film hardness, good heat resistance and outstanding anti-corrosion property.
Owner:SOUTH CHINA UNIV OF TECH

Jetting glue dispensing valve device and jetting glue dispensing method

The invention discloses a jetting glue dispensing valve device and a jetting glue dispensing method. The jetting glue dispensing valve device comprises a jetting glue dispensing valve, a glue supply pipeline and a glue supply valve, wherein a turntable capable of being closed / opened quickly is mounted at the bottom of the glue supply valve. During a glue jetting course, the glue supply valve is closed, and a channel allowing a glue solution to flow back to the glue supply valve from the glue supply pipeline is intercepted, so that glue jetting with precise volume is achieved. After a single glue jetting course is finished, the glue supply valve is opened, and the glue supply channel is opened for filling, so that continuous jetting of the glue solution is achieved. When the device and the jetting glue dispensing method are used for glue dispensing, no backflow occurs, so that an effective utilization rate of striker movement is increased, and jetting of a high-viscosity glue solution is facilitated; the device is simple in structure and easy to process; the turntable has the characteristic of periodic rotation, and can stir the glue solution, so that precipitation of fluorescent powder in the glue solution is avoided effectively; the fluid velocity in the jetting glue dispensing valve is distributed more uniformly; and the glue dispensing quality is ensured.
Owner:CENT SOUTH UNIV

Method and device for producing high-purity antimony

The invention relates to a method and device for producing high-purity antimony, and belongs to the field of high-purity non-ferrous metal metallurgy in the smelting industry. The method comprises the following technological steps: 1, putting needle antimony in a crucible, arranging the crucible into a vacuum tank, starting a water cooling system and a vacuum pump, and controlling the vacuity below 13 Pa; 2, controlling the bottom temperature of the crucible to between 600 and 900 DEG C, the medium temperature to between 500 and 650 DEG C and the top temperature to between 350 and 450 DEG C, and preserving the temperature for 1 to 3 hours; and 3, continuously raising the temperature of the bottom of the crucible to between 650 and 900 DEG C, volatilizing the antimony through holes, contacting the antimony with a conical titanium plate, condensing the antimony on the titanium plate, preserving the temperature to completely volatilize the antimony, and remaining impurities with high boiling point such as lead in the crucible. The method and the device have high production speed, low energy consumption and simple equipment processing, and are suitable for requirement of mass production. A water jacket is adopted for cooling, so the condensing effect is good; and the impurities are not refluxed basically, the purity of products is high, and the production process has no pollution and no pollutant emission.
Owner:株洲科迪亚实业有限公司

Low-temperature-resistant dispersing type sanitary sewage treatment integrated device and treatment method thereof

The invention provides a low-temperature-resistant dispersing type sanitary sewage treatment integrated device and a treatment method thereof. The low-temperature-resistant dispersing type sanitary sewage treatment integrated device comprises an adjusting tank, a first-stage anoxic tank, a first-stage aerobic tank, a second-stage anoxic tank, a second-stage aerobic tank, a third-stage anoxic tank, a third-stage aerobic tank, a secondary sedimentation tank, a solar heat collection system, a heat storage water tank and a heat exchanger. The adjusting tank is connected with the first-stage anoxic tank, the second-stage anoxic tank and the third-stage anoxic tank through a mechanical diaphragm metering pump and pipelines. The third-stage aerobic tank is connected with the secondary sedimentation tank. Filler is added to all stages of the aerobic tanks. Meanwhile, thermal insulation is conducted on a device shell, and heating is conducted through the solar heat collection system. The low-temperature-resistant dispersing type sanitary sewage treatment integrated device is small in occupied area, simple in operation, good in output water quality, convenient to maintain, low in operation cost, capable of being stably operated at a low temperature and capable of conducting dispersing type sanitary sewage integrated treatment.
Owner:沈阳工大蓝金环保产业技术研究院有限公司

UV (Ultraviolet) curable polyester as well as preparation method and application of UV curable polyester

The invention discloses UV (Ultraviolet) curable polyester as well as a preparation method and application of the UV curable polyester. The preparation method of the UV curable polyester comprises the following steps: 1) mixing 1 part of triglycidyl ether and 3 to 4 parts of an acrylic monomer into a reaction kettle according to a mole fraction; adding a quaternary ammonium salt catalyst, a polymerization inhibitor and an organic solvent and reacting at 105 DEG C to 125 DEG C until the acid value is less than 10mgKOH/g; 2) adding acid anhydride, a polymerization inhibitor and p-toluenesulfonic acid into a matrix prepared by the step 1), and reacting at 105 DEG C to 130 DEG C for 2h to 4h; adding an epoxy compound which is 0.9 to 1.2 times of the mole fraction of the acid anhydride and adding the quaternary ammonium salt catalyst and the organic solvent to react until the acid value is less than 10mgKOH/g; decompressing and distilling to remove the solvent, and cooling and discharging a material, wherein the solid content of the resin reaches 100 percent or more and the viscosity is 3000mPa.s to 30000mPa.s. UV curable paint prepared by the polyester has excellent coating film performance and relatively low cost.
Owner:SOUTH CHINA UNIV OF TECH

Rotary feeder sealed through air curtains

The invention provides a rotary feeder sealed through air curtains. The rotary feeder comprises a cambered impeller rotor, a shell body, a pressure limiting valve, a feeding inlet, a discharging outlet, rotating joints, externally-arranged bearings, big end caps, small end caps and conical sleeves. The cambered impeller rotor is of a hollow structure, and is provided with cambered plates evenly distributed along the circumference. An axial clearance taken as an airflow channel for the axial sealing air curtain is arranged between the tops of every two adjacent cambered plates. Annular clearances taken as airflow channels for the end face sealing air curtains are arranged between inner side plates and outer side plates. A hollow shaft, the cambered plates, the inner side plates and the outer side plates are connected into a whole. The cambered impeller rotor is detachably connected through the conical sleeves, studs, nuts, annular gaskets, arc-shaped grooves and the like. Compared with an existing feeder, the closed air curtains formed in the rotary feeder are good in sealing effect. The rotor does not make contact with the inner surface of the shell body, and the rotor is free of abrasion, so that the service life of parts and components is long. The rotor is flexible in operation and convenient to disassemble and clean. The rotary feeder can be taken as a non-contact rotary sealed feeding device which is capable of achieving continuous conveyance of materials.
Owner:CHANGZHOU UNIV

Direct-discharge water-saving pedestal pan with elastic water seal door by using water impact force

ActiveCN102094450AAvoid problems that are easy to block and affect useShort rinse timeWater closetsFlushing timeWater saving
The invention provides a direct-discharge water-saving pedestal pan with an elastic water seal door by using water impact force. In the invention, a horizontal water outlet is arranged on an outer end of a lower water port of a pelvic cavity ceramic main body; a downward bulge is arranged on the top end of a joint between the horizontal water outlet and the lower water port; and an elastic water seal door assembly is arranged on the horizontal water outlet and can reserve a sealing water level which is higher than the bulge in the horizontal water outlet under a balanced condition without an external force, and the elastic water seal door assembly is elastically and extensionally deformed to be opened under the action of the water impact force so that water and pollutants are rapidly discharged into a sewer. The pedestal pan or squat pan using the elastic water seal door device is very water-saving (1L of water is used in the case of low water mark and 3L of water is used in the case of high water mark), and is far superior to provisions of national and international water-saving standards; and the flushing time is very short, the pollutant backflow and peculiar smell are avoided, and 100% of sealed water is replaced, thus being beneficial to health and environmental protection, and effectively avoiding the problem that the traditional pedestal pan and squat pan are easily blocked to affect applications.
Owner:广东泰妮科技有限公司

Device and method for sealing, grouting, and reinforcing broken coal-rock masses

The invention belongs to the technical field of surrounding rock control in coal mining, and particularly relates to a device and method for sealing, grouting, and reinforcing broken coal-rock masses.Technical problems such as poor sealing and grouting effects and complex construction in the prior art are solved. The device mainly comprises a grouting pipe, a wrench, a nut, a casing pipe, a sealing sleeve, a gasket, a tail end joint, a duckbill valve, and a tail end protection tube, one end of the grouting pipe is provided with an external thread, the nut is in screw joint with the grouting pipe through the external thread, the wrench is connected to the outside of the nut in a sleeving mode, the other end of the grouting pipe is fixedly connected with the tail end joint, the tail end protection tube is fixed to the tail end joint, and the duckbill valve is mounted on the tail end joint in a sleeving mode and completely located in the protection tube at the tail end; and the casing pipe, the sealing sleeve and the gasket are mounted on the outer wall of the grouting pipe between the nut and the tail end joint in turn in a sleeving mode. According to the device and method for sealing, grouting, and reinforcing the broken coal-rock masses, the sealing effect is good, the grouting process is simple, slurry can be prevented from flowing back, the cost is low, the grouting speed ishigh, and the device for sealing, grouting, and reinforcing the soft and broken coal-rock masses can be widely used and promoted.
Owner:HENAN POLYTECHNIC UNIV

Medical centrifugal pump head

The invention relates to the technical field of medical treatment, and particularly relates to a medical centrifugal pump head. The medical centrifugal pump head comprises a pump shell and an inducer rotationally installed in the pump shell; a magnet is arranged at the bottom of the inducer; the pump shell is provided with a liquid inlet and a liquid push-out opening; a top positioning sleeve and a bottom positioning sleeve are arranged in the pump shell; a positioning rod capable of rotating around the inducer is arranged at the axis of the inducer, and the two ends of the positioning rod are respectively connected with the top positioning sleeve and the bottom positioning sleeve; the section of the liquid inlet is gradually increased in the liquid inflow direction, and the liquid inlet is located in the center of the top of the pump shell; a plurality of blades with inclined side surfaces are arranged on the inducer, and an angle between the liquid push-out opening and the blades is 45 degrees; and a plurality of positioning notches capable of being connected with external equipment are formed in the bottom of the pump shell. The medical centrifugal pump head adopts the bearing-free design, is less in friction and lower in heat production, ensures that no vortex exists in a liquid inlet and the liquid push-out opening of the centrifugal pump head, is uniform in acceleration, and keeps the optimal blood flow.
Owner:卡迪美科北京生物科技有限公司
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