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Modified asphalt storage stability standard viscosity detection method

A technology of storage stability and standard viscosity, applied in flow characteristics, measuring devices, instruments, etc., can solve problems such as large differences, waste of resources, and accelerated aging of modified asphalt, so as to improve test efficiency, save test materials, and improve utilization rate effect

Inactive Publication Date: 2016-05-04
NORTHWEST UNIVERSITY FOR NATIONALITIES
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  • Summary
  • Abstract
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  • Claims
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AI Technical Summary

Problems solved by technology

[0003] (1) The test conditions can not well simulate the actual storage conditions of modified asphalt, and the test temperature conditions are inconsistent with the actual conditions (the test conditions are 163 ° C ± 5 ° C oven heating for 48 ± 1 h, and then refrigerated in a sub-zero refrigerator for at least 4 hours before melting Do the storage stability segregation test, the actual modified asphalt storage temperature does not have such rapid cooling and rapid heating change process); 52 hours of test time, even if the test results are reliable, it can only guarantee the stability of the modified asphalt within 52 hours, and cannot guarantee storage Stable for more than 52 hours
[0004] ⑵Using aluminum tubes or glass test tubes as modified asphalt sample containers cannot be reused, which is a waste of resources, and glass test tubes are used to freeze for at least 4 hours and then smashed, which also increases the unsafe factors of the test environment
[0005] (3) The slenderness ratio of the test container does not match the geometric dimension ratio of the on-site asphalt storage equipment
[0006] (4) During the freezing process of the modified asphalt sample, the segregation speed of the modified asphalt slows down, which is quite different from the actual segregation process.
[0007] ⑸Using softening point analysis of modified asphalt storage stability test process requires repeated heating and cooling of modified asphalt (ie heating, freezing, heating, cooling, reheating), and the aging of modified asphalt is accelerated in the process of repeated heating. At the same time, repeated heating will prolong the test period and reduce the test efficiency. More importantly, the test cold and hot cycle process is inconsistent with the actual storage cold and hot process.
Does not reflect the actual storage stability well

Method used

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  • Modified asphalt storage stability standard viscosity detection method

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Embodiment Construction

[0022] Modified asphalt storage stability standard viscosity detection method, including the following steps:

[0023] (1) There are sample outlets at the bottom, 1 / 3 height, and 2 / 3 height of the stainless steel tube 2 with openings at both ends, and ball valves 1 are provided at the sample outlets (see figure 1 ).

[0024] Wherein: the inner diameter of the stainless steel pipe 2 is 40mm, and the length is 250mm.

[0025] (2) Close the ball valve 1 at the bottom of the stainless steel pipe 2 obtained in the step (1), open the ball valve 1 at the 21 / 3 height and 2 / 3 height of the stainless steel pipe; then heat the 200 ± 5g modified asphalt sample filtered through a 0.3mm sieve And pour into the stainless steel pipe 2.

[0026] (3) Put the stainless steel tube 2 obtained in step (2) into an oven, heat at 163°C±5°C for 48±1h, and then cool naturally to room temperature.

[0027] (4) Heat and melt the modified asphalt sample cooled to room temperature at 163°C±5°C; then, clo...

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Abstract

The invention relates to a modified asphalt storage stability standard viscosity detection method. The method comprises the following steps that 1, the bottom end, one-third height position and two-third height position of a stainless steel pipe with two open ends are provided sample outlets respectively, and the sample outlets are provided with ball valves; 2, the ball valve at the bottom end of the stainless steel pipe is turned off, and the ball valves at the one-third height position and two-third height position of the stainless steel pipe are turned on; a filtered modified asphalt sample is heated and poured into the stainless steel pipe; 3, the stainless steel pipe is placed into a drying oven to be heated for 48+ / -1 h, and then naturally cooled to indoor temperature; 4, the modified asphalt sample cooled to indoor temperature is heated and molten again; by adjusting the ball valves to be turned on or off, the upper one-third part of the modified asphalt is injected into a standard viscosity test instrument for standard viscosity testing, and the lower one-third part of the modified asphalt is injected into a standard viscosity test instrument for standard viscosity testing; the two results are compared, and therefore the stability can be analyzed. The modified asphalt storage stability standard viscosity detection method is accurate in result and high in efficiency.

Description

technical field [0001] The invention relates to the technical field of modified asphalt testing, in particular to a standard viscosity detection method for storage stability of modified asphalt. Background technique [0002] At present, the following defects exist in the modified asphalt segregation test: [0003] (1) The test conditions can not well simulate the actual storage conditions of modified asphalt, and the test temperature conditions are inconsistent with the actual conditions (the test conditions are 163 ° C ± 5 ° C oven heating for 48 ± 1 h, and then refrigerated in a sub-zero refrigerator for at least 4 hours before melting Do the storage stability segregation test, the actual modified asphalt storage temperature does not have such rapid cooling and rapid heating change process); 52 hours of test time, even if the test results are reliable, it can only guarantee the stability of the modified asphalt within 52 hours, and cannot guarantee storage Stable for more...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N11/00
CPCG01N11/00
Inventor 王秀芳张常安
Owner NORTHWEST UNIVERSITY FOR NATIONALITIES
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