Preparation method of chemical nickel-plating solution
A technology of electroless nickel plating and preparation method, which is applied in the direction of liquid chemical plating, metal material coating process, coating, etc., and can solve the problem of nickel plating solution scrapping, solution stability is not high, and electroless nickel plating scrap solution treatment process is complicated and other problems, to achieve the effect of fine electroless nickel plating and good bonding force
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Embodiment 1
[0021] A kind of preparation method of electroless nickel plating solution, process condition is as follows:
[0022] (1) Inject 1 / 3 volume of pure water into the nominal roughening tank, add sulfuric acid according to the technical requirements of 1ml / L concentration, and then add acetic acid according to the technical requirements of 1ml / L concentration, adjust the pH to 1.5, and finally use Fill the roughening tank with pure water to the volume required by the process, then heat the solution in the tank to 40°C, and seal it for later use.
[0023] (2) Inject 1 / 3 volume of pure water into the nominally good sensitization tank, add stannous chloride according to the technical requirements of a concentration of 5g / L, then add hydrochloric acid according to the technical requirements of a concentration of 1ml / L, and finally use pure water Fill the roughening tank with the volume required by the process, then heat the solution in the tank to 40°C, and seal it for later use.
[...
Embodiment 2
[0028] A kind of preparation method of electroless nickel plating solution, process condition is as follows:
[0029] (1) Inject 1 / 3 volume of pure water into the nominal roughening tank, add sulfuric acid according to the technical requirements of the concentration of 3ml / L, then add acetic acid according to the technical requirements of the concentration of 3ml / L, adjust the pH to 2.0, and finally use Fill the roughening tank with pure water to the volume required by the process, then heat the solution in the tank to 45°C, and seal it for later use.
[0030] (2) Inject 1 / 3 volume of pure water into the nominal sensitization tank, add stannous chloride according to the technical requirements of 8g / L concentration, then add hydrochloric acid according to the technical requirements of 2ml / L concentration, and finally use pure water Fill the roughening tank with the volume required by the process, then heat the solution in the tank to 50°C, and seal it for later use.
[0031] (...
Embodiment 3
[0034] A kind of preparation method of electroless nickel plating solution, process condition is as follows:
[0035] (1) Inject 1 / 3 volume of pure water into the nominal roughening tank, add sulfuric acid according to the technical requirements of a concentration of 5ml / L, and then add acetic acid according to the technical requirements of a concentration of 5ml / L, adjust the pH to 2.5, and finally use Fill the roughening tank with pure water to the volume required by the process, then heat the solution in the tank to 55°C, and seal it for later use.
[0036] (2) Inject 1 / 3 volume of pure water into the nominal sensitization tank, add stannous chloride according to the technical requirements of concentration 10g / L, then add hydrochloric acid according to the technical requirements of 3ml / L concentration, and finally use pure water Fill the roughening tank with the volume required by the process, then heat the solution in the tank to 55°C, and seal it for later use.
[0037] ...
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