Device for removing bubbles in pitch through vacuum auxiliary temperature differential method and bubble removing method thereof

A vacuum-assisted, temperature-difference method, applied in filament forming treatment, textile and papermaking, fiber treatment, etc., can solve the problems of inability to realize industrial application, unsuitability, and hindering the development of pitch-based carbon fiber continuous filament preparation technology.

Active Publication Date: 2016-08-03
湖南东映碳材料科技有限公司
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  • Abstract
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  • Application Information

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Problems solved by technology

However, there are the following deficiencies: firstly, this method is mainly used in analytical experiments in the petrochemical industry, and cannot be applied industrially; in addition, it is mainly aimed at the degassing of asphalt with low softening point and low viscosity, and is not suitable for the degassing of asphalt with high softening p

Method used

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  • Device for removing bubbles in pitch through vacuum auxiliary temperature differential method and bubble removing method thereof

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Effect test

Embodiment 1

[0026] This embodiment is a specific implementation of the present invention, specifically the following steps:

[0027] Step 1: Connect the degassing kettle 2 and the buffer tank 5, and evacuate to 100Pa, close the communication valve 1 4 and the communication valve 2 6 between the two, stop vacuuming, and pass inert gas into the degassing kettle 2 , by adjusting the 3 valves of the intake pipeline to keep the normal pressure in the degassing tank, heat the asphalt in the tank to 320°C, and stir the asphalt with a stirrer for 2 hours;

[0028] Step 2: Stop stirring, close the valve 3 of the intake pipeline, open the connecting valve 1, and gradually cool down to 50°C below the softening point of the asphalt. At this time, the bubbles crack, and continue to vacuumize the degassing kettle 2, the pressure is 50Pa, and the time is 2h;

[0029] Step 3: Raise the temperature of the defoaming tank 2 to 340°C, and continue to carry out negative pressure sedimentation treatment on th...

Embodiment 2

[0033] This embodiment is a specific implementation of the present invention, specifically the following steps:

[0034] Raise the heating temperature of the asphalt in step 1 in Example 1 to 350°C, and extend the stirring time to 4h; reduce the temperature in step 2 to 100°C below the softening point of the asphalt, and appropriately extend the negative pressure treatment time to 4h; The temperature in the medium was raised to 365°C, and the pressure was dropped to 5kPa, and the settling time was extended to 15h.

[0035] The air bubble removal rate can reach 99.9%, and the continuous length of the spinnable asphalt can reach more than 4km.

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Abstract

The invention discloses a device for removing bubbles in pitch through a vacuum auxiliary temperature differential method and a bubble removing method thereof. The device comprises a bubble removing kettle and a buffering tank and further comprises a heating part used for supplying heat to the bubble removing kettle, a pitch soaking stirrer, an inert gas inlet pipeline and a vacuum pump system, the bubble removing kettle and the buffering tank are communicated through a first communicating valve, a waste discharge valve is connected to the bottom of the buffering tank, and the buffering tank and the vacuum pump system are communicated through a second communicating valve. The temperature differential method is introduced into a traditional bubble removing method, medium and low molecules in pitch are volatilized fully at a high temperature by means of stirring, the temperature is reduced below the pitch softening point, the characteristic that an bubble film is easy to crack when being converted into the solid state from the liquid state is utilized, low-molecule volatile matter is drawn in a vacuum mode, and then temperature raising vacuum auxiliary sedimentation treatment is adopted for removing a small quantity of residual bubbles. The bubble removing rate can reach 99.9%, and pitch fiber with the size larger than 4 km can be spun continuously and stably.

Description

technical field [0001] The invention belongs to the technical field of pitch-based carbon fiber pitch spinning, and in particular relates to a device and method for removing air bubbles in pitch by a vacuum-assisted temperature difference method, which is used for the melting of mesophase pitch, a key process in the preparation of pitch-based carbon fiber continuous filaments. Pre-spinning treatment for spinning. Background technique [0002] Due to the wide molecular weight distribution of asphalt, the low molecular weight volatile matter vaporizes at the spinning temperature to form fine air bubbles, which will cause filament breakage during spinning. Therefore, removing the air bubbles in the molten asphalt is the key to ensure smooth spinning and stable carbon filament quality. Pre-spinning treatment. At present, there are mainly three methods for asphalt melting and degassing, namely, static degassing method, pressurized degassing method and vacuum degassing method. Am...

Claims

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Application Information

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IPC IPC(8): D01D1/10
CPCD01D1/103
Inventor 李轩科叶崇李保六黄东
Owner 湖南东映碳材料科技有限公司
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