A kind of method for preparing cocoa butter
A technology of cocoa butter and kernel fat, applied in the field of oil processing, can solve the problem that cocoa butter-like cocoa butter cannot be well compatible, and achieve the effect of good compatibility and high yield
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Embodiment 1
[0031] Mix candle fruit oil and palm olein at a ratio of 4:6, and then form a mixed oil with acetone at a ratio of 1:5; heat the mixed oil to 40°C at a stirring speed of 55r / min to destroy all crystals in the system; the first Fraction extraction, at a stirring speed of 30r / min, the temperature of the mixed oil was lowered to 20°C at a cooling rate of 3.0°C / min, crystallized at a constant temperature for 5 hours, and the stearin was separated by vacuum filtration to obtain a mixed oil from which the stearin was removed; The second fraction is extracted, under the stirring speed of 8r / min, the temperature of the mixed oil after removing the stearin is lowered to 8°C at a cooling rate of 1.5°C / min, crystallized at a constant temperature for 7h, and the liquid oil is separated by distillation under reduced pressure, and the obtained hard Fat vacuum distillation recovery solvent, which is rich in symmetrical triglyceride cocoa butter, its 2-oleic acid-1,3-dipalmitic acid glyceride,...
Embodiment 2
[0033] Evenly mix Michelin and palm oil at a ratio of 8:2, and then form a mixed oil with n-hexane at a ratio of 8:1; at a stirring speed of 75r / min, raise the temperature of the mixed oil to 45°C to destroy all crystals in the system; One-stage fractionation, at a stirring speed of 30r / min, lower the temperature of the mixed oil to 8°C at a cooling rate of 2.5°C / min, crystallize at a constant temperature for 5 hours, and separate the stearin by suction filtration under reduced pressure to obtain a stearin-removed mixed oil ; The second fraction is extracted, at a stirring speed of 7r / min, the temperature of the mixed oil after stearin removal is reduced to -5°C at a cooling rate of 1.0°C / min, crystallized at a constant temperature for 6h, and the liquid oil is separated by vacuum distillation, The resulting stearin is distilled under reduced pressure to recover the solvent, which is cocoa butter-like mainly containing symmetrical triglycerides, including 2-oleic acid-1,3-dipal...
Embodiment 3
[0035] Mix mango kernel butter and palm oil evenly at 8:2, and then form a mixed oil with n-hexane at 6:1; heat the mixed oil to 45°C at a stirring speed of 70r / min to destroy all crystals in the system; the first Fraction extraction, at a stirring speed of 22r / min, the temperature of the mixed oil was lowered to 10°C at a cooling rate of 3.5°C / min, crystallized at a constant temperature for 5 hours, and the stearin was separated by vacuum filtration to obtain a mixed oil from which the stearin was removed; For the second fraction extraction, at a stirring speed of 8r / min, the temperature of the mixed oil after removal of stearin was lowered to -5°C at a cooling rate of 1.5°C / min, crystallized at a constant temperature for 5.5h, and the liquid oil was separated by distillation under reduced pressure. Gained stearin is distilled under reduced pressure to recover the solvent, which is cocoa butter-like mainly containing symmetrical triglycerides; the third fraction is extracted, ...
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