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Cs2lipo4 compound, cs2lipo4 nonlinear optical crystal and its preparation method and application
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A nonlinear optics and compound technology, applied in nonlinear optics, phosphorus compounds, chemical instruments and methods, etc., can solve the problems of small birefringence, easy deliquescence of CLBO, large birefringence, etc., and achieve stable physical and chemical properties, Large nonlinear optical effect, good mechanical properties
Active Publication Date: 2018-04-10
FUJIAN INST OF RES ON THE STRUCTURE OF MATTER CHINESE ACAD OF SCI
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For example, the birefringence of LBO is relatively small, and the quadrupling output of 1064nm wavelength laser cannot be realized; the birefringence of BBO is relatively large, and there is a photorefractive effect when used for quadrupling output of 1064nm wavelength laser, which limits its Output power and beam quality; while CLBO is extremely deliquescent and difficult to achieve commercial applications; KBBF is difficult to obtain crystals with a large c-thickness due to its serious layered growth habit
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Embodiment 1
[0052] Adopt solid phase reaction method, reaction equation is as follows:
[0053] Cs 2 CO 3 +LiOH·H 2 O+NH 4 h 2 PO 4 =Cs 2 LiPO 4 ↑+CO 2 ↑+3H 2 O↑+NH 3 ↑
[0054] The dosages of the above three reagents are respectively: Cs 2 CO 3 1.629g (0.005mol), LiOH·H 2 O 0.209 g (0.005 mol), NH 4 h 2 PO 4 0.575g (0.005mol).
[0055] The specific operation steps are: weigh the reagents according to the above dosages, put them into a mortar, mix and grind them evenly, then put them into a corundum ceramic crucible, compact them, put them into a muffle furnace, and heat them at 10°C / Heat up to 400°C at a rate of 1 hour, then heat-preserve and sinter for more than 12 hours, take it out and grind it evenly after cooling down to room temperature, then heat it up to 600°C at a rate of 10°C / hour and sinter for more than 24 hours, take it out and grind it for more than 1 time in the middle, that is, pure Phase Cs 2 LiPO 4 compound.
[0056] Such as figure 2 As shown, t...
Embodiment 2
[0058] Preparation of powdered Cs 2 LiPO 4 compound
[0059] Adopt solid phase reaction method, reaction equation is as follows:
[0062] 0.02mol CsNO 3 , 0.005mol Li 2 CO 3 , 0.01mol (NH 4 ) 2 HPO 4 .
[0063] The specific operation steps are: weigh the reagents according to the above dosage, put them into a mortar, mix and grind them evenly, then put them into a corundum ceramic crucible, compact them, put them into a muffle furnace, and heat them at 200 ° C / Heat up to 450°C at a rate of 1 hour, then heat-preserve and sinter for more than 12 hours, take it out and grind it evenly after cooling down to room temperature, then heat up to 650°C at a rate of 200°C / hour and sinter for more than 24 hours, take it out and grind it for more than 1 time in the middle, that is, pure Phase Cs 2 LiPO 4 compou...
Embodiment 3～10
[0065] Embodiment 3~10 is to prepare Cs 2 LiPO 4 the crystal
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Abstract
The invention relates to a Cs2LiPO4 compound and Cs2LiPO4 nonlinear optical crystal as well as a preparation method and application thereof. The crystal provided by the invention is easy to grow, is transparent and free of inclusion, and has the advantages of being relatively rapid in growing speed, low in cost, easy in preparing crystal of relatively large size, and the like. The prepared crystal has the advantages of being relatively short in ultraviolet absorption cut-off side, relatively great in nonlinear optical effect, stable in physical and chemical stability, good in mechanical property, easy in processing and the like; the crystal can be used to manufacture nonlinear optical devices; the nonlinear optical devices made of the nonlinear optical crystal can be used in multiple military and civil high-tech fields such as laser blind weapons, optical disc record, laser projection televisions, optical calculation and optical fiber communication.
Description
technical field [0001] The present invention relates to a kind of Cs 2 LiPO 4 Compound, Cs 2 LiPO 4 Nonlinear Optical Crystals, Cs 2 LiPO 4 Crystal preparation method, Cs 2 LiPO 4 Use of crystals for making nonlinear optical devices and containing Cs 2 LiPO 4 Optical devices for nonlinear optical crystals. Background technique [0002] The nonlinear optical effect of crystal refers to such an effect: when a beam of laser light with a certain polarization direction passes through a nonlinear optical crystal in a certain direction, the frequency of the beam will change. Crystals with nonlinear optical effects are called nonlinear optical crystals. Using the nonlinear optical effect of crystals, nonlinear optical devices such as second harmonic generators, up-down frequency converters, and optical parametric oscillators can be made. The all-solid-state laser using nonlinear optical crystals for frequency conversion is a development direction of lasers in the future, ...
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Patent Type & Authority Patents(China)
IPC IPC(8): C30B29/14C30B11/00C01B25/45G02F1/355
CPCC01B25/45C30B11/00C30B29/14G02F1/3551
Inventor 罗军华沈耀国赵三根赵炳卿
Owner FUJIAN INST OF RES ON THE STRUCTURE OF MATTER CHINESE ACAD OF SCI
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