A kind of preparation method of high elastic luminous elastic fabric
A high-elasticity, fabric technology, applied in chemical instruments and methods, luminescent materials, textiles and papermaking, etc., can solve the problems of poor wearing comfort, hard hand feel, unable to maintain the elastic requirements of elastic fabrics, and achieve color fastness to friction. Excellent washing fastness and dry hand feeling
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Embodiment 1
[0029] Example 1 A method for preparing a highly elastic luminous stretch fabric, comprising the following process steps:
[0030] (1) Synthesis of highly elastic polyurethane prepolymer: Distill 115g of polyoxypropylene glycol and 146g of polytetrahydrofuran ether polyol in a reaction kettle under reduced pressure (vacuum degree 67mmHg) for 0.6~1 hour, and control the temperature at 60~100°C Next, remove traces of water in advance. 115g of polyoxypropylene glycol, 146g of polytetrahydrofuran ether polyol, 40.6g of toluene diisocyanate, 46.5g of xylylene diisocyanate, and 20.9g of dimethylol butyric acid after vacuum distillation were put into a nitrogen protection In the reaction kettle, mix and stir evenly, heat up to 70°C, and the reaction time is 4h, then add 2.8g of γ-aminopropyltriethoxysilane, adjust the temperature, keep the temperature at 55°C, and keep it warm for 2h to prepare High elastic polyurethane prepolymer.
[0031] (2) Preparation of high-elastic polyureth...
Embodiment 2
[0035] Example 2 A method for preparing a highly elastic luminous stretch fabric, comprising the following process steps:
[0036] (1) Synthesis of highly elastic polyurethane prepolymer: 105g of polyoxypropylene triol and 153g of polytetrahydrofuran ether polyol were distilled under reduced pressure (vacuum degree 67mmHg) in a reaction kettle for 1h, and the temperature was controlled at 100°C to remove traces of of water. Put 105g of polyoxypropylene glycol, 153g of polytetrahydrofuran ether polyol, 43.3g of toluene diisocyanate, 47.8g of xylylene diisocyanate, and 22.5g of dimethylol butyric acid after vacuum distillation into a nitrogen-protected In the reaction kettle, mix and stir evenly, heat up to 85°C, and the reaction time is 3h, then add 2.7g of γ-aminopropyltriethoxysilane, adjust the temperature, keep the temperature at 65°C, and keep it warm for 2h to prepare High elastic polyurethane prepolymer.
[0037] (2) Preparation of high-elastic polyurethane emulsion: t...
Embodiment 3
[0041] Example 3 A method for preparing a highly elastic luminous stretch fabric, comprising the following process steps:
[0042] (1) Synthesis of highly elastic polyurethane prepolymer: 130g of polyoxypropylene triol and 189g of polytetrahydrofuran ether polyol were distilled under reduced pressure (vacuum degree 67mmHg) in a reaction kettle for 0.8h, and the temperature was controlled at 80°C. Trace amounts of water. Put 130g of polyoxypropylene glycol, 189g of polytetrahydrofuran ether polyols, 46.8g of toluene diisocyanate, 37.2g of xylylene diisocyanate, and 23g of dimethylol butyric acid after vacuum distillation into a nitrogen-protected In the reaction kettle, mix and stir evenly, heat up to 80°C, and the reaction time is 3.5h, then add 2.5g of γ-aminopropyltriethoxysilane, adjust the temperature, keep the temperature at 60°C, and keep it warm for 2h to prepare High elastic polyurethane prepolymer.
[0043](2) Preparation of high-elastic polyurethane emulsion: the t...
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