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Temperature control system and temperature control sample stage for atomic force microscope

An atomic force microscope and sample stage technology, applied in the field of sample stage, can solve the problems of long time consumption, high energy consumption, inaccurate temperature adjustment, etc., and achieve the effects of precise target temperature control, low energy consumption, and quick temperature adjustment.

Inactive Publication Date: 2017-02-22
NANJING UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Regardless of whether it is indoors or in a sealed box, because there is too much space to adjust the temperature, it takes a long time to adjust the temperature to the target temperature, and the temperature adjustment is not accurate enough, and the energy consumption is high

Method used

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  • Temperature control system and temperature control sample stage for atomic force microscope
  • Temperature control system and temperature control sample stage for atomic force microscope

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0017] This embodiment is a temperature-controlled sample stage for an atomic force microscope, such as figure 1 , figure 2 As shown, it includes a table top 11 , a sample pool 12 and a temperature control chamber 13 . The table top 11 is a circular disk structure with a diameter of 6-10 cm. The sample cell 12 is arranged on the table top 11 and is a structure surrounded by a ring above the table top 11 . A temperature measuring probe 21 is fixed in the sample pool 12 . The temperature measuring probe 21 is externally connected with a temperature measuring connector 31 . In this embodiment, the temperature measuring probe 21 is fixed in the sample cell 12 by pasting.

[0018] The temperature control chamber 13 is located under the table top 11 and is a chamber located under the sample pool 12 . Specifically, the temperature control chamber 13 is a structure surrounded by a circular body with a side opening 132 under the platform 11 . The diameter of the torus surroundin...

Embodiment 2

[0024] This embodiment is a temperature control system for an atomic force microscope, such as figure 2 As shown, a temperature measuring and controlling instrument 41 , a peristaltic pump 42 and the temperature-controlled sample stage for an atomic force microscope in Embodiment 1 are shown. The temperature measurement and control instrument 41 is connected to the temperature measurement probe 21 and the semiconductor temperature control chip 22 through the temperature measurement joint 31 and the temperature control joint 32 respectively. The peristaltic pump 42 is connected to the cooling coil 23 through the water inlet joint 331 and the water outlet joint 332 .

[0025] The temperature measuring and controlling instrument 41 is a sample cell temperature controller made of a single-chip microcomputer, and is used to control the temperature in the sample cell 12 . Specifically, the temperature measuring and controlling instrument 41 obtains the temperature in the sample ce...

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PUM

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Abstract

The invention discloses a temperature control system and a temperature control sample stage for an atomic force microscope. The temperature control sample stage comprises a stage panel, a sample pool and a temperature control chamber. The sample pool is arranged on the stage panel, and a temperature measurement joint is externally connected with a temperature measurement probe which is fixed in the sample pool. The temperature control chamber is arranged below the stage panel and is a cavity under the sample pool, and a semiconductor temperature control piece and a heat radiation coil are arranged in the temperature control chamber. The semiconductor temperature control piece is externally connected with a temperature control joint, and a water inlet joint and a water outlet joint are externally connected with the heat radiation coil. The temperature control system comprises a temperature measurement and control instrument, a peristaltic pump and the temperature control sample stage. The temperature measurement and control instrument is connected with the temperature measurement probe and the semiconductor temperature control piece, and the peristaltic pump is connected with the heat radiation coil. Due to a small size of the sample pool, quickness and convenience in temperature adjustment, precision in target temperature control and low energy consumption are realized.

Description

technical field [0001] The invention relates to an accessory under an atomic force microscope, in particular to a sample stage capable of regulating the temperature of a sample pool under the atomic force microscope. Background technique [0002] The atomic force microscope is a widely used scientific research instrument for observing the molecular-level properties of the sample surface and performing single-molecule force spectroscopy experiments. Temperature is a very important environmental factor when using AFM, since single-molecule force spectroscopy data are related to ambient temperature. Under the prior art, the ambient temperature control of the atomic force microscope is realized by controlling the large ambient temperature. For example, place the atomic force microscope in a room with adjustable temperature, or place the atomic force microscope in a sealed box with adjustable temperature. Regardless of the room or the sealed box, because there is too much space...

Claims

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Application Information

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IPC IPC(8): G01Q30/10
CPCG01Q30/10
Inventor 李鹏飞曹毅王炜
Owner NANJING UNIV
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