Ceramic binder, ceramic-metal composite material and preparation method thereof, composite material setter

A technology of ceramic binder and composite material, which is applied in the field of superhard material product manufacturing, can solve the problems of large temperature difference between the upper and lower sides of the ceramic setter, uneven product performance, and inability to guarantee accuracy, so as to prevent oxidation deformation and improve the success rate of sintering , making convenient effects

Active Publication Date: 2019-02-22
FUNIK ULTRAHARD MATERIAL
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Graphite plate has good thermal conductivity, but it is easy to oxidize at high temperature, the accuracy cannot be guaranteed, and its service life is short. At the same time, it is easy to generate carbon monoxide, carbon dioxide and other gases in the sintering furnace, which is not conducive to sintering
[0004] The corundum-mullite setter plate is currently the most used ceramic setter plate, which has the advantage of not being easily oxidized. For example, the Chinese invention patent with the publication number CN102674864A discloses a corundum-mullite setter plate formula: it is made of electrofused Mollite Come stone, fused white corundum, tabular corundum, a-A1 2 o 3 It is composed of fine powder, kaolin, activator, and binder, but its thermal conductivity is poor, and the temperature difference between the upper and lower ceramic setters is large, which makes the performance of the product uneven.

Method used

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  • Ceramic binder, ceramic-metal composite material and preparation method thereof, composite material setter

Examples

Experimental program
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Effect test

Embodiment 1

[0030] The vitrified bond in this embodiment is made up of the following mass percentage components: 60% SiO 2 , 20% Al 2 o 3 , 7% H 3 BO 3 , 8% MgO, 4% Na 2 CO 3 , 1% CaF 2 .

[0031] The ceramic-metal composite material in this embodiment is made of the following raw materials in mass percentage: 32% of the above-mentioned ceramic bond, 8% of nickel-chromium alloy, 58% of white corundum, and 2% of water glass.

[0032] The ceramic-metal composite material is a composite material setter.

[0033] The preparation method of the composite material setter in the present embodiment: comprises the steps:

[0034] 1) Mix the vitrified bond, nickel-chromium alloy, white corundum, and water glass to obtain the mixture, put the mixture into the mold, and use 100kg / cm 2 The pressure was maintained for 30s and pressed into shape, and after demoulding, it was put into an oven and dried at 80°C for 24 hours to obtain a blank; the particle size of the nickel-chromium alloy was 320 ...

Embodiment 2

[0038] The vitrified bond in this embodiment is made up of the following components by mass percentage: 50% SiO 2 , 25% Al 2 o 3 , 10% H 3 BO 3 , 6% MgO, 8% Na 2 CO 3 , 1% CaF 2 .

[0039] The ceramic-metal composite material in this embodiment is made of the following raw materials in mass percentage: 25% of the above vitrified bond, 10% of nickel-chromium alloy, 60% of alumina, and 5% of water glass.

[0040]The preparation method of the ceramic-metal composite material in the present embodiment: comprises the following steps:

[0041] 1) Mix the vitrified bond, nickel-chromium alloy, aluminum oxide, and water glass to obtain the mixture, put the mixture into the mold, and use 50kg / cm 2 The pressure is kept under pressure for 20s and pressed into shape, and after demoulding, put it into an oven and dry it for 20 hours at 100°C to obtain a blank; the particle size of the nickel-chromium alloy is 300 mesh, and the particle size of alumina is 300 mesh;

[0042] 2) Put ...

Embodiment 3

[0044] The vitrified bond in this embodiment consists of the following components by mass percentage: 65% SiO 2 , 15% Al 2 o 3 , 8% H 3 BO 3 , 5% MgO, 5% Na 2 CO 3 , 2% CaF 2 .

[0045] The ceramic-metal composite material in this embodiment is made of the following raw materials in mass percentage: 35% of the above-mentioned ceramic bond, 5% of nickel-chromium alloy, 59% of white corundum, and 1% of water glass.

[0046] The preparation method of the ceramic-metal composite material in the present embodiment: comprises the following steps:

[0047] 1) Mix the vitrified bond, nickel-chromium alloy, white corundum, and water glass to obtain the mixture, put the mixture into the mold, and use 75kg / cm 2 The pressure was maintained for 45s and pressed into shape, and after demolding, put it into an oven and dry it at 90°C for 22 hours to obtain a blank; the particle size of the nickel-chromium alloy was 400 mesh, and the particle size of the white corundum was 400 mesh;

...

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Abstract

The invention discloses a ceramic binder, a ceramic metal composite material and a preparing method of the ceramic metal composite material and a composite material load bearing board, and belongs to the technical field of super-hard material product manufacturing. The ceramic binder is prepared from, by mass, 50%-70% of SiO2, 15%-25% of Al2O3, 5%-10% of H3BO3, 5%-10% of MgO, 3%-8% of Na2CO3 and 1%-2% of CaF2, the raw materials are simple in ingredients, the binding strength is high, and the ceramic binder is stable at high temperature. The composite material load bearing board is prepared from, by mass, 25%-35% the ceramic binder, 5%-10% of metal binder, 55%-65% of aluminium oxide or white corundum and 1%-5% of sodium silicate. The composite material load bearing board well matches ceramic inorganic substances with metal, achieves ideal heat transfer speed, and stabilizes performance of a sintered product.

Description

technical field [0001] The invention relates to a vitrified bond, a ceramic-metal composite material and a preparation method thereof, and a composite material setter plate, belonging to the technical field of superhard material product manufacturing. Background technique [0002] The sintering process of superhard materials is divided into hot-press sintering and cold-press sintering. Hot-press sintering is carried out at the same time as heating and pressure during sintering. Hot-press sintered products have less porosity, high density and stable performance, but the number of sintering at one time is small, Low production efficiency and high production cost. Cold-press sintering is free sintering under no pressure. Cold-press sintering products have the advantages of high porosity, good sharpness, large number of sintering at one time, low production cost, and are suitable for the production and processing of special-shaped products. They are more and more popular in prod...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C03C10/16C22C29/12C22C1/05C22C1/10
CPCC03C10/16C22C1/051C22C29/005C22C29/12
Inventor 杨德涛
Owner FUNIK ULTRAHARD MATERIAL
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