High dielectric constant microwave dielectric material added with strontium oxide and preparation method and application thereof
A technology of microwave dielectric material and strontium oxide, which is applied in the field of electronic information, can solve the problems that devices cannot work stably, and achieve the effect of facilitating industrial mass production, moderate sintering temperature and high dielectric constant
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Embodiment 1
[0025] In the embodiment of the present invention, a high dielectric microwave dielectric material added with strontium oxide has a general formula of Ba 0.75 (Li 0.5 SM 0.5 ) 0.25 ZrO 3 +0.06wt.%SrO.
[0026] The preparation method of the high dielectric microwave dielectric material added with strontium oxide comprises the following steps:
[0027] (1) Accurately weigh analytically pure BaCO according to the general formula 3 , Li 2 CO 3 、Sm 2 o 3 , ZrO 2 , SrO, mixed, with zirconia balls as the medium, absolute ethanol as the solvent, powder: zirconia balls: absolute ethanol=1g: 3g: 1.5ml, wet ball milling for 16h, the slurry obtained was dried, passed 60 mesh sieves to obtain mixed powder;
[0028] (2) Pre-sinter the mixed powder at a temperature of 1000°C in an air atmosphere for 5 hours;
[0029] (3) Add absolute ethanol to the pre-sintered mixed powder as a medium, wet ball mill again for 16 hours, dry the obtained slurry, pass through an 80-mesh sieve, and ...
Embodiment 2
[0033] In the embodiment of the present invention, a high dielectric microwave dielectric material added with strontium oxide has a general formula of Ba 0.85 (Li 0.5 SM 0.5 ) 0.15 ZrO 3 +0.08wt.%SrO.
[0034] The preparation method of the high dielectric microwave dielectric material added with strontium oxide comprises the following steps:
[0035] (1) Accurately weigh analytically pure BaCO according to the general formula 3 , Li 2 CO 3 、Sm 2 o 3 , ZrO 2 , SrO, mixed, with zirconia balls as the medium, absolute ethanol as the solvent, powder: zirconia balls: absolute ethanol=1g: 4g: 1.2ml, wet ball milling for 20h, the obtained slurry was dried, passed 60 mesh sieves to obtain mixed powder;
[0036] (2) Pre-sinter the mixed powder at a temperature of 1050°C in an air atmosphere for 3 hours;
[0037] (3) Add absolute ethanol to the pre-sintered mixed powder as a medium, wet ball mill again for 20 hours, dry the obtained slurry, pass through a 80-mesh sieve, and o...
Embodiment 3
[0041] In the embodiment of the present invention, a high dielectric microwave dielectric material added with strontium oxide has a general formula of Ba 0.78 (Li 0.5 SM 0.5 ) 0.22 ZrO 3 +0.065wt.%SrO.
[0042] The preparation method of the high dielectric microwave dielectric material added with strontium oxide is the same as that in Example 1.
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