A high-efficiency melt-spinning method for low-damping polymers
A technology of melt spinning and low damping, applied in the direction of conjugated synthetic polymer rayon, one-component polyester rayon, one-component polyamide rayon, etc., which can solve the lack of melt rheological resistance Necessary considerations and other issues to achieve the effect of low surface energy and simple installation
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Embodiment 1
[0054] A method for high-efficiency melt spinning of low-damping polyethylene terephthalate short fibers. First, a polysiloxane treatment liquid is prepared. First, 10 parts by weight have a pH value of 10.1 and a solid content of 30 wt%. The average particle diameter is the alkaline silica sol of 30nm and 10 parts of pH value are 9.4, and solid content is 20wt%, and the basic aluminum sol of average particle diameter is 45nm to mix, then add 5 parts of formic acid as catalyst adjustment system pH value, make pH value is maintained at 2, then add 10 parts of mixed solvent of ethanol and water, the volume ratio of ethanol and water is 1.25:1, then add 30 parts of methyltrimethoxysilane, then carry out hydrolysis at normal temperature for 15min, and then put Put the system at 45°C for high-temperature condensation, and keep the reaction for 30 minutes. After the reaction, add 1 part of the mixture of leveling agent BYK 310, defoamer BYK 025 and surface hardening and wear-resistan...
Embodiment 2
[0065]A method for high-efficiency melt spinning of low-damping polyethylene terephthalate short fibers. First, a polysiloxane treatment solution is prepared. First, 20 parts by weight have a pH value of 10.5 and a solid content of 45 wt%. The average particle diameter is the alkaline silica sol of 50nm and 20 parts of pH values are 9.8, solid content is 35wt%, and the basic aluminum sol of average particle diameter is 65nm to mix, then add 8 parts of acetic acid as catalyst adjustment system pH value, make pH value is maintained at 4.5, then add 20 parts of isopropanol and water mixed solvent, the volume ratio of isopropanol and water is 1.42:1, then add 40 parts of methyltriethoxysilane, and then hydrolyze at room temperature 20min, then put the system at 80°C for high-temperature condensation, and keep the reaction for 75min. After the reaction, add 3 parts of leveling agent BYK 310, defoamer BYK 025 and surface hardening resistance Abrasive T801 mixture additive, after s...
Embodiment 3
[0076] A method for high-efficiency melt spinning of low-damping polytrimethylene terephthalate short fibers. First, a polysiloxane treatment solution is prepared. First, 15 parts by weight of The alkaline silica sol with a diameter of 40nm and 15 parts of alkaline aluminum sol with a pH value of 9.6, a solid content of 30wt%, and an average particle diameter of 50nm are mixed, and then 6 parts of hydrochloric acid are added as a catalyst to adjust the pH value of the system to maintain the pH value. In 3, then add 15 parts of butanol and water mixed solvent, the volume ratio of butanol and water is 1.60:1, then add 35 parts of ethyltriethoxysilane, then carry out hydrolysis at normal temperature for 18min, and then Put the system at 50°C for high-temperature condensation, and keep the reaction for 40 minutes. After the reaction, add 2 parts of BYK 310 leveling agent, BYK 025 defoamer and T801 surface hardening and wear-resistant agent with a mass ratio of 1:1:0.25. Mixture ad...
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