Linear rotating type sample inlet moving device for carbon tetrachloride monitoring instrument and work method of linear rotating type sample inlet moving device
A technology of carbon tetrachloride and moving device, which is applied in the field of linear rotary sample feeding moving device of carbon tetrachloride monitor, can solve the problems of small application range and unfavorable sample detection, etc., and achieve reduced labor intensity, high operating efficiency, The effect of high degree of equipment automation
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Embodiment 1
[0052] Manufacture clamping plate 7-6-3 of the present invention according to the following steps, and in parts by weight:
[0053]Step 1: Add 3,400 parts of ultrapure water with a conductivity of 5.43μS / cm into the reactor, start the stirrer in the reactor at a speed of 86rpm, start the heating pump, and raise the temperature in the reactor to 87°C; add in sequence 65 parts of 4-(3-chloro-2-pyrazine)-1,4-piperidinedicarboxylic acid 1-(1,1-dimethylethyl) 4-methyl ester, 3-hydroxy-4-[( 182 parts of 2-methyl-5-nitrophenyl)azo]-N-phenyl-2-naphthylcarboxamide, 4-[4-amino-2-(hydroxymethyl)phenyl]-1-piper 234 parts of 1,1-dimethylethyl pyridinecarboxylate, stirred until completely dissolved, adjusted the pH value to 6.6, adjusted the speed of the agitator to 139rpm, and the temperature was 115°C, and the esterification reaction was carried out for 28 hours;
[0054] Step 2: Take 212 parts of 2,2-bis[(nonanoyloxy)methyl]-1,3-propane(alcohol) dinonanoic acid, 5-benzyl-hexahydropyrrol...
Embodiment 2
[0059] Manufacture clamping plate 7-6-3 of the present invention according to the following steps, and in parts by weight:
[0060] Step 1: Add 4210 parts of ultrapure water with a conductivity of 8.35μS / cm into the reactor, start the stirrer in the reactor at a speed of 163rpm, start the heating pump, and raise the temperature in the reactor to 128°C; add in sequence 98 parts of 4-(3-chloro-2-pyrazine)-1,4-piperidinedicarboxylic acid 1-(1,1-dimethylethyl) 4-methyl ester, 3-hydroxy-4-[( 2-methyl-5-nitrophenyl)azo]-N-phenyl-2-naphthylcarboxamide 241 parts, 4-[4-amino-2-(hydroxymethyl)phenyl]-1-piper 316 parts of 1,1-dimethylethyl pyridine carboxylic acid, stirred until completely dissolved, adjusted the pH value to 9.2, adjusted the speed of the agitator to 189 rpm, and the temperature was 151 ° C, and the esterification reaction was carried out for 40 hours;
[0061] Step 2: Take 325 parts of 2,2-bis[(nonanoyloxy)methyl]-1,3-propane(alcohol) dinonanoic acid, 5-benzyl-hexahydr...
Embodiment 3
[0066] Manufacture clamping plate 7-6-3 of the present invention according to the following steps, and in parts by weight:
[0067] Step 1: Add 3,800 parts of ultrapure water with a conductivity of 6.89μS / cm into the reactor, start the stirrer in the reactor at a speed of 126rpm, start the heating pump, and raise the temperature in the reactor to 108°C; add in sequence 81 parts of 4-(3-chloro-2-pyrazine)-1,4-piperidinedicarboxylic acid 1-(1,1-dimethylethyl) 4-methyl ester, 3-hydroxy-4-[( 2-methyl-5-nitrophenyl)azo]-N-phenyl-2-naphthylcarboxamide 211 parts, 4-[4-amino-2-(hydroxymethyl)phenyl]-1-piper 275 parts of 1,1-dimethylethyl pyridine carboxylic acid, stirred until completely dissolved, adjusted the pH value to 7.9, adjusted the speed of the agitator to 164 rpm, and the temperature was 134 ° C, and the esterification reaction was carried out for 34 hours;
[0068] Step 2: Take 268 parts of 2,2-bis[(nonanoyloxy)methyl]-1,3-propane(alcohol) dinonanoic acid, 5-benzyl-hexahyd...
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