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Adsorbing type reaction device for organic synthesis

A reaction equipment and organic synthesis technology, applied in the field of adsorption-type reaction equipment, can solve the problems of odor, strong odor, etc., and achieve the effect of controlling emissions

Active Publication Date: 2017-11-17
CHENGDU ORGANOCHEM CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The technical problem to be solved by the present invention is that odor is generated during the reaction of organic matter, and the purpose is to provide adsorption reaction equipment for organic synthesis to solve the problem of strong odor generated by organic synthesis

Method used

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  • Adsorbing type reaction device for organic synthesis

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] Such as figure 1 As shown, the present invention is used for the adsorption type reaction equipment of organic synthesis, comprises kettle body 1, and the upper bottom surface of described kettle body 1 is heat insulation board 2, and the lower bottom surface of kettle body 1 is heat conduction plate 3, and heat insulation board 2 and The heat conduction plate 3 seals the kettle body 1, and the cavity between the heat insulation plate 2 and the heat conduction plate 3 is a reaction chamber 4, and the top of the heat insulation plate 2 is connected with a box body 5 with a solid air freshener inside, and the box body 5 A first heating cover 6 with a heating device inside is connected above the top of the heat conduction plate 3, a second heating cover with a heating device inside is connected under the heat conduction plate 3, and a conduit 7 communicating with the inside of the box body 5 is connected to the side of the box body 5 , the conduit 7 is connected to the rea...

Embodiment 2

[0025] Based on embodiment 1, the inside of the chamber wall of the reaction chamber 4 is provided with a condensation chamber 9 with condensed water, the chamber wall of the reaction chamber 4 is an adiabatic chamber wall, and the condensation chamber 9 is located at the top of the reaction chamber 4 .

[0026] The condensation chamber is used to condense the gas at the top of the reaction chamber, which is conducive to the recovery of reactants such as volatilized organic solvents, improves the conversion rate of organic synthesis, and can also reduce the emission of organic matter.

Embodiment 3

[0028] Based on the above embodiment, the port of the conduit 7 inside the reaction chamber 4 is provided with a grid-like baffle 10 on the side close to the inside of the reaction chamber 4 , and the grid-shaped baffle 10 completely covers the port surface of the conduit 7 .

[0029] The grid-shaped baffle can not only play the role of filtration, but also play the role of condensing and guiding liquid. After the steam generated in the reaction chamber hits the grid-shaped baffle, part of the steam will condense into liquid and return to the reaction chamber. Continue to react.

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Abstract

The invention discloses an adsorbing type reaction device for organic synthesis. The adsorbing type reaction device comprises a kettle, wherein a heat insulating plate is arranged on the upper bottom surface of the kettle; a heat conducting plate is arranged on the lower bottom surface of the kettle; the heat conducting plate and the heat insulating plate are used for sealing the kettle; a chamber between the heat conducting plate and the heat insulating plate is arranged as a reaction chamber; a box which is filled with a solid air refresher is connected with the upper side of the heat insulating plate; a first heating cover in which a heating device is arranged is connected with the upper side of the box; a second heating cover in which the heating device is arranged is connected with the lower side of the heat conducting plate; a guide pipe which is connected with the interior of the box is connected with a side wall of the box; the guide pipe is connected with the reaction chamber; an organic matter absorbing net is arranged in a port of the guide pipe connected with the reaction chamber; and an exhaust port is formed on the guide pipe. According to the invention, the odor is covered by the air refresher and the content of the organic matter in air is reduced at the benefit aspect, so that the problem of strong odor caused by organic synthesis is solved.

Description

technical field [0001] The invention relates to a reaction kettle, in particular to adsorption reaction equipment for organic synthesis. Background technique [0002] Organic synthesis is roughly divided into two aspects: (1) Basic organic synthesis: including the synthesis of important chemical industrial raw materials from raw materials such as coal, petroleum, water and air, such as raw materials for synthetic fibers, plastics and synthetic rubber, solvents, plasticizers, gasoline etc., its output is almost close to the order of magnitude of steel; (2) Fine organic synthesis: including the synthesis of more complex molecular compounds from simpler raw materials, such as chemical reagents, medicines, pesticides, dyes, spices and detergents. [0003] A large amount of organic matter is involved in organic synthesis, and most organic solvents will volatilize. Therefore, a strong odor will be emitted during most organic synthesis reactions. The odor will not only adversely af...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01J19/24B01D53/02B01D53/00
CPCB01D53/002B01D53/02B01D2257/90B01J19/24
Inventor 谈平忠谈平安周永恒陈军
Owner CHENGDU ORGANOCHEM CO LTD
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