Injectable gel material for spinal repair
A gel material, spine technology, applied in medical science, prosthesis, etc., can solve the problem of inability to assess the safety of degradation and metabolism, and achieve the effect of increasing strength, promoting response, and improving sustainability
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Embodiment 1
[0025] An injectable gel material for spinal repair, characterized in that: the preparation method of the gel material follows the steps:
[0026] Step 1, adding single-arm PEG into deionized water, stirring evenly, adding barium sulfate dispersant to prepare PEG aqueous solution;
[0027] Step 2, the HAuCl 4 Add deionized water to prepare gold-containing aqueous solution;
[0028] Step 3: Slowly add the gold-containing aqueous solution into the PEG aqueous solution, and stir well to obtain a dynamic hydrogel solution, which is the gel material.
[0029] The one-arm PEG in the step 1 adopts thiol-terminated 4-arm poly(ethylene glycol).
[0030] The molecular weight of the one-arm PEG in the step 1 is 2000.
[0031] The concentration of PEG in the step 1 is 25%.
[0032] The content of the barium sulfate in the said step 1 is 15%.
[0033] HAuCl of the gold-containing aqueous solution in the step 2 4 The concentration is 0.2M.
[0034] The volume ratio of the PEG aqueous...
Embodiment 2
[0036] An injectable gel material for spinal repair, characterized in that: the preparation method of the gel material follows the steps:
[0037] Step 1, adding single-arm PEG into deionized water, stirring evenly, adding barium sulfate dispersant to prepare PEG aqueous solution;
[0038] Step 2, the HAuCl 4 Add deionized water to prepare gold-containing aqueous solution;
[0039] Step 3: Slowly add the gold-containing aqueous solution into the PEG aqueous solution, and stir well to obtain a dynamic hydrogel solution, which is the gel material.
[0040] The one-arm PEG in the step 1 adopts thiol-terminated 4-arm poly(ethylene glycol).
[0041] The molecular weight of the one-arm PEG in the step 1 is 3000.
[0042] The concentration of PEG in the step 1 is 40%.
[0043] The content of barium sulfate in the described step 1 is 25%.
[0044] HAuCl of the gold-containing aqueous solution in the step 2 4 The concentration is 0.3M.
[0045] The volume ratio of the PEG aqueou...
Embodiment 3
[0047] An injectable gel material for spinal repair, characterized in that: the preparation method of the gel material follows the steps:
[0048] Step 1, adding single-arm PEG into deionized water, stirring evenly, adding barium sulfate dispersant to prepare PEG aqueous solution;
[0049] Step 2, the HAuCl 4 Add deionized water to prepare gold-containing aqueous solution;
[0050] Step 3: Slowly add the gold-containing aqueous solution into the PEG aqueous solution, and stir well to obtain a dynamic hydrogel solution, which is the gel material.
[0051] The one-arm PEG in the step 1 adopts thiol-terminated 4-arm poly(ethylene glycol).
[0052] The molecular weight of the one-arm PEG in the step 1 is 2500.
[0053] The concentration of PEG in the step 1 is 30%.
[0054] The content of barium sulfate in the described step 1 is 20%.
[0055] HAuCl of the gold-containing aqueous solution in the step 2 4 The concentration is 0.25M.
[0056] The volume ratio of the PEG aqueo...
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