Preparation method and application of in-situ nitrogen-doped carbon microsphere adsorbent
A microsphere adsorption, nitrogen and carbon technology, applied in chemical instruments and methods, adsorption water/sewage treatment, other chemical processes, etc., can solve the problems of poor universality, small adsorption capacity, slow adsorption rate of water treatment adsorbents, etc. Achieve the effect of solving the bottleneck problem, large adsorption capacity and broad market application prospects
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specific Embodiment approach 1
[0038] Specific embodiment 1: This embodiment is a method for preparing an in-situ nitrogen-doped carbon microsphere adsorbent, which is specifically prepared according to the following steps:
[0039] 1. Synthesis of nitrogen-containing polymer microspheres:
[0040] ①. Add a buffer and a nitrogen-containing polymer monomer to the ethanol solution to obtain a reaction solution; then use a hydrogen chloride aqueous solution with a concentration of 100 mmol / L to 200 mmol / L to adjust the pH of the reaction solution to 7.5 to 9 to obtain the pH value A reaction solution with a pH of 7.5-9; the reaction solution with a pH of 7.5-9 is reacted at a temperature of 20°C to 40°C and a rotation speed of 50r / min-100r / min for 36h-72h to obtain a reaction product;
[0041] The volume ratio of absolute ethanol to water in the ethanol solution described in step 1 ① is 1:(3-8);
[0042] The concentration of the nitrogen-containing polymer monomer in the reaction solution described in step 1 ① is 1 g / ...
specific Embodiment approach 2
[0060] Embodiment 2: The difference between this embodiment and Embodiment 1 is that the shielding gas in step 2 is nitrogen or argon, and the flow rate of the shielding gas is 100 mL / min to 300 mL / min. The other steps are the same as in the first embodiment.
specific Embodiment approach 3
[0061] Specific embodiment three: This embodiment is different from specific embodiment one or two in that the protective gas in step three is nitrogen or argon, and the flow rate of the protective gas is 100 mL / min to 300 mL / min. The other steps are the same as the first or second embodiment.
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