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High-throughput hydrothermal synthesis and surface treatment device

A surface treatment device, hydrothermal synthesis technology, applied in chemical/physical processes, chemical/physical/physical chemical processes, chemical instruments and methods, etc., can solve the problem of slow cooling speed, inability to ensure the accuracy of temperature control, and difficult to meet The uniformity of the heating of the reactor and other issues can be achieved to save time, reduce the impact, and evenly heat the effect

Pending Publication Date: 2018-05-11
SOUTHWEST JIAOTONG UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, most hydrothermal synthesis reactors are heated by electric drying ovens, which is difficult to meet the heating uniformity of each reactor
At the same time, with the electric heating drying box cooling or taking out the air cooling, the cooling speed is slow, and the accuracy of temperature control cannot be guaranteed

Method used

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  • High-throughput hydrothermal synthesis and surface treatment device
  • High-throughput hydrothermal synthesis and surface treatment device
  • High-throughput hydrothermal synthesis and surface treatment device

Examples

Experimental program
Comparison scheme
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Embodiment Construction

[0021] The present invention will be further described below in conjunction with the accompanying drawings and specific embodiments.

[0022] Such as Figure 1-3 As shown, a high-throughput hydrothermal synthesis and surface treatment device includes a device body 1 and a heating and cooling treatment device 3 arranged in the device body 1; the heating and cooling treatment device 3 includes an upper cover 31, a bottom cover 33 and The heat insulation part 32 arranged between the upper cover 31 and the bottom cover 33; the heat insulation part 32 is provided with a plurality of heat conduction sleeves 5, and the heat conduction sleeve 5 is provided with a hydrothermal reaction synthesis kettle 4; Cooling water pipes 6 and electric furnace wires 7 are wound on the surface; both cooling water pipes 6 and electric furnace wires 7 are connected to a temperature control device.

[0023] Further, the device body 1 is a box structure, and is provided with a box door 2 .

[0024] Fu...

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PUM

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Abstract

The invention discloses a high-throughput hydrothermal synthesis and surface treatment device. The device comprises a device body and heating and cooling treatment devices arranged in the device body,wherein each heating and cooling treatment device comprises an upper cover, a bottom cover and a thermal insulation part arranged between the upper part and the bottom cover, a plurality of thermal conduction sleeves are arranged inside the thermal insulation part, and a hydrothermal synthesis reaction kettle is arranged in each thermal conduction sleeve; the outer surface of each thermal conduction sleeve is wound with a cooling water pipe and an electric stove wire; the cooling water pipes and the electric stove wires are both connected with temperature control devices. Cooling circulationof the cooling water pipe and heating of the electric stove wire outside each thermal conduction sleeve are controlled through the temperature control devices, each hydrothermal synthesis reaction kettle can be heated and cooled separately, and the high-throughput requirement can be realized.

Description

technical field [0001] The invention relates to a hydrothermal synthesis and surface treatment device, in particular to a high-throughput hydrothermal synthesis and surface treatment device. Background technique [0002] The hydrothermal method, also known as the high-temperature solution method, refers to an effective method for inorganic synthesis and material preparation in a special sealed pressure reactor, using a solution as the reaction system, and heating the reaction system to generate a high-temperature and high-pressure environment. Methods; there is no equipment in the hydrothermal reactor that can simultaneously react at different temperatures and meet mass production; at present, high-throughput preparation of materials is an important part of the work of materials genome, and its characteristic is that in the material preparation process, Realize the simultaneous preparation of different formula components; the existing hydrothermal synthesis and surface treat...

Claims

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Application Information

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IPC IPC(8): B01J3/04B01J19/00
CPCB01J3/04B01J19/0013B01J2219/00094
Inventor 翁杰李兴许韬韬杨杰何磊郭泰林鲁雄段可
Owner SOUTHWEST JIAOTONG UNIV
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