Pore forming agent removal method of battery diaphragm and preparation process of lithium ion secondary battery diaphragm
A preparation process and secondary battery technology, which is applied to battery components, circuits, electrical components, etc., can solve the problems of thick substrate extraction difficulties, achieve the effects of shortening extraction time, solving extraction difficulties, and accelerating extraction rates
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[0027] Example one
[0028] A method for removing a pore-forming agent of a battery diaphragm, which is applied to the preparation process of a lithium ion secondary battery diaphragm. The steps of the method include:
[0029] The diaphragm substrate is pretreated by the equipment to remove at least a part of the pore former in the diaphragm substrate in advance; in this embodiment, the pore former is white oil, but it is not limited to this; when the white oil is at 40°C, the kinematic viscosity 45-55mm 2 / s;
[0030] The pre-processed diaphragm substrate is extracted by ultrasonic extraction to extract the pore-forming agent and ensure that the residual rate of the pore-forming agent in the final battery diaphragm is less than 1%.
[0031] In the ultrasonic extraction process, the ultrasonic frequency is 17KHz, and the ultrasonic extraction time is 10min.
[0032] The equipment includes a scraping roller set with at least one pair of scraping rolls 1 and a vacuum suction device with ...
Example Embodiment
[0045] Example two
[0046] This embodiment is basically the same as the first embodiment, except that during the ultrasonic extraction process, the ultrasonic frequency is 28KHz, and the ultrasonic extraction time is 10 minutes.
Example Embodiment
[0047] Example three
[0048] This embodiment is basically the same as the first embodiment, except that during the ultrasonic extraction process, the ultrasonic frequency is 17KHz, and the ultrasonic extraction time is 15min.
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