Radix acanthopanax total flavonoid injection and method for extracting radix acanthopanax total flavonoid from radix acanthopanax senticosus

A technology of Acanthopanax ginseng and Acanthopanax senticosus, which is applied in the field of extraction and application of plant components, can solve problems such as potential safety hazards of Acanthopanax senticosus injection, achieve good medicinal activity, improve utilization rate, and reduce raw material costs

Inactive Publication Date: 2018-07-10
大连军门保健食品有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

Therefore, when intravenous infusion of drugs containing potassium ions, the concentration of potassium ions generally does not exceed 0.3%, but the Acanthopanax injection on the market does not pay attention to the concentration of potassium ions, so that there is a certain safety in Acanthopanax injection Hidden danger

Method used

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  • Radix acanthopanax total flavonoid injection and method for extracting radix acanthopanax total flavonoid from radix acanthopanax senticosus
  • Radix acanthopanax total flavonoid injection and method for extracting radix acanthopanax total flavonoid from radix acanthopanax senticosus

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0045] A method for extracting total flavonoids of Acanthopanax senticosus from Radix Acanthopanax, the steps are as follows:

[0046] Step a, five ginseng raw material pretreatment:

[0047] a1: Select fresh raw materials of Wujiaginseng, clean them and dry them in a vacuum drying oven at 60-65°C for 10-15 hours, and crush the fully dried raw materials of Wujiaginseng into 50-100 meshes;

[0048] a2: Add petroleum ether to the Wujiashen powder obtained in step a1, the mass volume ratio of the Wujiashen powder to petroleum ether is 1g:5-10mL, reflux and extract for 2-3h, filter and remove the filtrate, and put the filter residue into Dry in a vacuum oven at 50°C for 30 minutes to volatilize the solvent, and obtain the defatted Wujiaginseng powder from which the fat-soluble impurities in the chlorophyll have been removed;

[0049] Step b, high-pressure extraction of the total flavonoids of Acanthopanax senticosus in defatted Acanthopanax ginseng powder:

[0050] b1: Add 40% e...

Embodiment 2

[0061] A method for extracting total flavonoids of Acanthopanax from Radix Acanthopanax is as follows:

[0062] Step a, five ginseng raw material pretreatment:

[0063] a1: Select fresh leaves of Wujiaginseng, clean them, dry them in a vacuum oven at 60°C for 10 hours, and crush the fully dried Wujiaginseng raw materials to 50 meshes;

[0064] a2: Add petroleum ether to the Wujiashen powder obtained in step a1, the mass volume ratio of the Wujiashen powder to petroleum ether is 1g:5mL, reflux and extract for 2 hours, filter and remove the filtrate, and put the filter residue at 50°C for vacuum drying Dry in the box for 30 minutes to volatilize the solvent, and obtain the defatted Wujiaginseng powder from which the fat-soluble impurities in the chlorophyll have been removed;

[0065] Step b, high-pressure extraction of the total flavonoids of Acanthopanax senticosus in defatted Acanthopanax ginseng powder:

[0066] b1: Add 40% ethanol solution to the degreased Acanthopanax po...

Embodiment 3

[0080] A method for extracting the total flavonoids of Acanthopanax Radix from Radix Acanthopanax Radix is ​​as follows:

[0081] Step a, five ginseng raw material pretreatment:

[0082] a1: Select fresh ginseng flowers, clean them and dry them in a vacuum drying oven at 62°C for 12 hours, and crush the fully dried ginseng raw materials to 80 meshes;

[0083]a2: Add petroleum ether to the Wujiashen powder obtained in step a1, the mass volume ratio of the Wujiashen powder to petroleum ether is 1g:6mL, filter and remove the filtrate after reflux extraction for 3 hours, and put the filter residue at 50°C for vacuum drying Dry in the box for 30 minutes to volatilize the solvent, and obtain the defatted Wujiaginseng powder from which the fat-soluble impurities in the chlorophyll have been removed;

[0084] Step b, high-pressure extraction of the total flavonoids of Acanthopanax senticosus in defatted Acanthopanax ginseng powder:

[0085] b1: Add 40% ethanol solution to the degrea...

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Abstract

The invention belongs to the field of plant ingredient extraction and application, and particularly relates to a radix acanthopanax total flavonoid injection and a method for extracting radix acanthopanax total flavonoid from radix acanthopanax senticosus. A high-pressure extraction process is used for extracting the radix acanthopanax total flavonoid from the radix acanthopanax senticosus; a polyamide resin and macroporous adsorption resin separation and purification process is used for further purifying the radix acanthopanax total flavonoid. The separation extraction method is performed atroom temperature; the destroy on medicine active ingredients is reduced; the obtained extract has better medicinal activity; the extraction time is short; the efficiency is high; the operation is simple and convenient; the energy sources are saved; the environment pollution is little; the yield and the purity of the radix acanthopanax total flavonoid are high; the method can be used for industriallarge batch production. The radix acanthopanax total flavonoid injection prepared by using the adix acanthopanax total flavonoid extracted from the radix acanthopanax senticosus by the extraction method as raw materials has the advantages of low undue toxicity, high safety, stable quality and high effective ingredient activity.

Description

technical field [0001] The invention belongs to the field of extraction and application of plant components, and in particular relates to an injection of Acanthopanoate flavonoids and a method for extracting Acanthopanax Radix total flavonoids from Acanthopanax ginseng. Background technique [0002] Acanthopanax, also known as Siberian ginseng, Acanthopanax, etc., is a plant of the genus Araliaceae, and is a traditional precious medicinal plant in my country. It is mainly distributed in Heilongjiang, Jilin, Liaoning, Hebei and other places in China. Acanthopanax ginseng tastes pungent, slightly bitter, warm in nature, and non-toxic. It has the effects of nourishing qi and invigorating the spleen, nourishing the kidney and calming the nerves, and strengthening the bones. Using five ginseng to treat coronary heart disease can effectively relieve angina pectoris, and it also has the function of regulating blood pressure. In addition, five ginseng can also be used for leukopeni...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A61K36/254A61K9/08A61P9/10A61P25/00
CPCA61K9/0019A61K9/08A61K36/254A61K2236/333A61K2236/35A61K2236/37A61K2236/51A61K2236/53A61K2236/55
Inventor 黄仕研黄诗曼黄樱环
Owner 大连军门保健食品有限公司
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