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Method for rapidly dispersing conductive carbon black

A conductive carbon black, dispersion technology, applied in the direction of carbon preparation/purification, fibrous filler, etc., to achieve the effect of cost saving and rapid dispersion

Inactive Publication Date: 2018-10-12
河北宇轩纳米科技有限责任公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, there is no effective dispersion method for conductive carbon black in China, so it is of great significance to study the method of rapid dispersion without destroying the physical and chemical properties of conductive carbon black to maximize the advantages of conductive carbon black in materials.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0020] Weigh 20 parts of conductive carbon black with a certain mass, add 50 parts of deionized aqueous solution at 65°C, turn on the electric mixer for stirring, the initial speed is 250r / min, after fully dissolving, adjust the speed to 500r / min, and continue stirring for 15min , add 0.7 parts of dispersant, 0.4 parts of anti-sedimentation agent, and stir evenly.

Embodiment 2

[0022] Weigh 10 parts of conductive carbon black of a certain quality, add 30 parts of ethanol solution at 80°C, turn on the electric mixer for stirring at a speed of 350r / min, and ultrasonically 5 minutes after fully dissolving, add 0.5 parts of dispersant and 0.2 parts of stabilizer, and stir Evenly.

Embodiment 3

[0024] Weigh 40 parts of a certain mass of conductive carbon black, add 60 parts of isopropanol solution at 80°C, start the electric mixer to stir, the initial speed is 300r / min, after fully dissolved, disperse for 10min with a disperser, add wetting agent 0.5 portion, and stir well.

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PUM

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Abstract

The invention relates to a method for rapidly dispersing conductive carbon black. The method comprises the steps of adding a certain amount of conductive carbon black to a container,and adding a hot solution to the conductive carbon black; dispersing the conductive carbon black in the hot solution by a physical dispersion method,adding chemical additives simultaneously,and stirring and mixing thesolution and the chemical additives uniformly to finally obtain a uniform and stable conductive carbon black dispersion. The method combines physical and chemical dispersion to rapidly dissolve and disperse the conductive carbon black in a normal pressure vaporized molecular atmosphere,vaporize small molecules are separated among conductive carbon black aggregates,the distance during the vaporization processes is sharply increased to generate large expansion force which destroys the van der Waals force of the conductive carbon black aggregate,depolymerization is achieved,and the conductive carbon black is subjected to stabilization treatment by adding the chemical additives,thereby finally achieving the rapid dissolution and uniform dispersion of the conductive carbon black. The method caneffectively inhibit the agglomeration of the conductive carbon black and improve the dispersibility and stability of the conductive carbon black in a medium.

Description

technical field [0001] The invention relates to a method for quickly dispersing conductive carbon black, which belongs to the technical field of new materials. Background technique [0002] Conductive carbon black has the characteristics of high conductivity, high structural properties, irregular aggregates and very small size (nanoscale), large and rough specific surface area, clean surface (less compounds), and easy mixing with other materials. It can be effectively Form a three-dimensional network structure in the insulator, effectively improve the conductivity, and can endow the product with conductivity or antistatic effect. Conductive carbon black is the product with the best effect, the lowest cost, and the least likely to cause deterioration of the physical properties of the product among all conductive fillers. Conductive carbon black can be divided into conductive channel black (cc), conductive furnace carbon black (CF), superconductive furnace carbon black (SCF),...

Claims

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Application Information

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IPC IPC(8): C01B32/05C09C1/48
CPCC09C1/48C01B32/05
Inventor 高晓晔宋晋吴洪鹏侯林艳耿晓欣孟英
Owner 河北宇轩纳米科技有限责任公司