Method for quantitatively characterizing pores in shale
A quantitative characterization, pore technology, applied in measurement devices, permeability/surface area analysis, suspension and porous material analysis, etc., can solve the problems of not really revealing the actual size of shale pores, expensive, and difficult to operate.
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[0035] The present invention will be described in further detail below.
[0036] A method for quantitative characterization of pores in shale, comprising the steps of:
[0037] S1: Sample pretreatment and optical film preparation: For the collected shale samples, inject epoxy resin under high-pressure vacuum state, pay attention to control the pressure during injection to ensure that the shale samples are destroyed, and then inject epoxy resin The shale sample is ground into a laser confocal optical sheet, which requires an optical sheet size of about 1mm in thickness, or even thinner, with an area of 3×2cm or 3×3cm;
[0038] S2: Two-dimensional laser slice scanning and identification of pores in shale: 2D laser scanning was performed on the confocal laser slice prepared in S1 with a step size of 1.33 um and a resolution of 400 Hz to obtain a series of 2D Laser sectioning (that is, two-dimensional laser confocal micrographs); secondly, since the pores in shale are mainly comp...
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