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A method of measuring carbon roasting temperature by using petroleum coke lc value

A technology of petroleum coke and carbon, applied in the field of temperature measurement of carbon roasting furnace, can solve the problems of long measurement period, increased fluctuation of production process, complicated operation, etc., and achieve the effect of improving roasting effect, simplifying detection method and saving cost.

Active Publication Date: 2020-12-29
SUNSTONE DEV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Relying on manual experience control will easily lead to increased fluctuations in the production process, and abnormal product quality indicators such as resistivity, compressive strength, and flexural strength.
The cost of thermocouple testing is high and the measurement period is long. Due to the limitation of the furnace type, the actual heat treatment temperature of the middle and lower positions of the roasting furnace and the middle and lower electrodes cannot be measured. At the same time, the operation is complicated, so it is impossible to scientifically determine the heat treatment degree of the thermal kiln
The method of controlling according to the lattice size Lc value of the reference coke cannot accurately exclude different batches of raw materials because the sulfur content and trace metal elements affect the lattice size Lc value of the reference coke during the roasting process. The coke needs to be raw petroleum coke from the same origin and the same batch, and is prepared in batches at one time (CN 102109825A)

Method used

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  • A method of measuring carbon roasting temperature by using petroleum coke lc value

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0032] Utilize petroleum coke Lc value to measure the method of carbon roasting temperature:

[0033] 1) Select the reference petroleum coke, the crushed particle size is less than 5mm, screen to remove the powder, dry the others, stir evenly, select a certain range of particle size, analyze the indicators of carbonaceous materials, and set aside.

[0034] 2) The reference petroleum coke prepared in the above step 1) was heat-treated six times in the laboratory at a temperature gradient of 700°C, 800°C, 900°C, 1000°C, 1100°C, and 1200°C. For each heat treatment, the reference petroleum coke was rapidly heated to a controlled temperature, kept at this temperature for 2 h and then quenched immediately. Then use the diffraction method to measure their Lc value, draw the relationship curve and fitting equation between Lc value and temperature.

[0035] 3) Before the carbon to be roasted is loaded into the roaster, place the graphite container containing the reference petroleum co...

Embodiment 2

[0039] Utilize petroleum coke Lc value to measure the method of carbon roasting temperature:

[0040] 1) Select the reference petroleum coke, the crushed particle size is less than 5mm, screen to remove the powder, dry the others, stir evenly, select a certain range of particle size, analyze the indicators of carbonaceous materials, and set aside.

[0041] 2) The reference petroleum coke prepared in the above step 1) was heat-treated six times in the laboratory at a temperature gradient of 700°C, 800°C, 900°C, 1000°C, 1100°C, and 1200°C. For each heat treatment, the reference petroleum coke was rapidly heated to a controlled temperature, kept at this temperature for 2 h and then quenched immediately. Then use the diffraction method to measure their Lc value, draw the relationship curve and fitting equation between Lc value and temperature.

[0042] 3) Before the carbon to be roasted is loaded into the roaster, place the graphite container containing the reference petroleum co...

Embodiment 3

[0046] Utilize petroleum coke Lc value to measure the method of carbon roasting temperature:

[0047] 1) Select the reference petroleum coke, the crushed particle size is less than 5mm, screen to remove the powder, dry the others, stir evenly, select a certain range of particle size, analyze the indicators of carbonaceous materials, and set aside.

[0048] 2) The reference petroleum coke prepared in the above step 1) was heat-treated six times in the laboratory at a temperature gradient of 700°C, 800°C, 900°C, 1000°C, 1100°C, and 1200°C. For each heat treatment, the reference petroleum coke was rapidly heated to a controlled temperature, kept at this temperature for 2 h and then quenched immediately. Then their Lc values ​​were determined by diffractometry, and the relationship between Lc value and temperature and the fitting equation were drawn.

[0049] 3) Before the carbon to be roasted is loaded into the roasting furnace, place the graphite container containing the refere...

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Abstract

The invention discloses a method for measuring the roasting temperature of carbon by using the Lc value of petroleum coke, and belongs to the technical field of roasting temperature control of carbon. This method takes the equivalent temperature method as the main basis to calculate the equivalent roasting temperature, and at the same time corrects and eliminates the influence of the sulfur element, and does not need to redraw the relationship curve and fitting equation between the Lc value and the roasting temperature when the raw material is replaced, thereby improving Quickly and accurately obtain the equivalent roasting temperature. It overcomes the defects of technical adjustments based on the experience of operators, inaccurate measurement of the real furnace through direct placement of thermocouples, and high cost, and the control of the lattice size Lc value of the reference coke when replacing different batches of carbon to be roasted The defect that the reference petroleum coke needs to be replaced again when the raw material is used greatly simplifies the detection method. The detection window temperature range of the roasting furnace is 700°C to 1200°C, the roasting curve is optimized to improve the quality of the product, and the method is simple, fast and repeatable.

Description

technical field [0001] The invention relates to a method for measuring the temperature of a carbon roasting furnace, in particular to a method for measuring the carbon roasting temperature by using the Lc value of petroleum coke, and belongs to the technical field of carbon roasting temperature control. Background technique [0002] Petroleum coke is currently the main raw material for carbon production at home and abroad. It is a carbon material made of heavy residue produced after crude oil cracking through coking process, that is, thermal decomposition and polymerization (such as distillation, thermal distillation, thermal cracking, etc.). The element composition is mainly carbon, occasionally containing a small amount of sulfur, hydrogen, nitrogen, oxygen and some metal elements, sometimes with water. Widely used in metallurgy, chemical and other industries as electrodes or raw materials for the production of chemical products. [0003] The heat treatment process of pet...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N23/20G01K13/00
CPCG01K13/00G01N23/20
Inventor 黎文湘高守磊蒋金龙郝吉旺
Owner SUNSTONE DEV