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High-temperature rosin activated oil and manufacturing method thereof

A manufacturing method and technology of active oil, applied in dyeing method, natural resin refining, textile and papermaking, etc., can solve the problems of loss of use value, dry and brittle rosin, loss of activity, etc., achieve good anti-diffusion performance, improve utilization frequency, the effect of increasing activity

Active Publication Date: 2018-12-11
SHANDONG KEYSTONE LUBRICANT TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Under normal circumstances, rosin will become dry and brittle after a real wax printing and dyeing process, lose its activity, and thus lose its use value

Method used

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  • High-temperature rosin activated oil and manufacturing method thereof
  • High-temperature rosin activated oil and manufacturing method thereof

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0037] Basic components: 150BS bright oil: 100kg; hydrogenated rosin (additional, the same below): 20kg;

[0038] Functional additives (additional, the same below): anti-diffusion agent: 5kg; antioxidant: 0.5kg; wetting agent: 0.2kg; defoamer: 0.02kg.

[0039] During manufacturing:

[0040] 1) Measure and pump 60kg of 150BS bright stock to the first stirred tank, start stirring, and heat to 40-60°C;

[0041] 2) Measure and pump the remaining 150BS bright stock to the second stirring tank, start stirring, and heat to 80-85°C;

[0042] 3) Add 20kg of hydrogenated rosin and 0.5Kg of antioxidant into the second stirred tank, and mix evenly with 50kg of 150BS bright stock heated to 80-85°C with stirring;

[0043] 4) Pump the homogeneously mixed product in step 3) into the first stirred tank, then sequentially add 5 kg of anti-diffusion agent, 0.2 kg of wetting agent, and 0.02 kg of defoamer into the first stirred tank, and stir After mixing evenly, high-temperature rosin active ...

Embodiment 2

[0045] Basic components: 150BS bright oil: 100kg; hydrogenated rosin: 25kg;

[0046] Functional additives: anti-diffusion agent: 8kg; antioxidant: 1kg; wetting agent: 0.2kg; defoamer: 0.02kg.

[0047] During manufacturing:

[0048] 1) Measure and pump 60kg of 150BS bright stock to the first stirred tank, start stirring, and heat to 40-60°C;

[0049] 2) Measure and pump the remaining 150BS bright stock to the second stirring tank, start stirring, and heat to 80-85°C;

[0050] 3) Measure 25kg of hydrogenated rosin and 1.0Kg of diisooctyldiphenylamine into the second stirred tank, and mix evenly with 150BS bright stock heated to 80-85°C with stirring;

[0051] 4) Pump the uniformly mixed product in step 3) to the first stirred tank, then sequentially transport 8 kg of anti-diffusion agent, 0.2 kg of wetting agent, and 0.02 kg of defoamer to the first stirred tank, and stir and mix After homogenization, high-temperature rosin active oil is obtained.

Embodiment 3

[0053] Basic components: 150BS bright oil: 100kg; hydrogenated rosin: 30kg;

[0054] Functional additives: anti-diffusion agent: 10kg; antioxidant: 1.4kg; wetting agent: 0.28kg; defoamer: 0.03kg.

[0055] During manufacturing:

[0056] 1) Measure and pump 50kg of 150BS bright stock to the first stirred tank, start stirring, and heat to 40-60°C;

[0057] 2) Measure and pump the remaining 150BS bright stock to the second stirring tank, start stirring, and heat to 80-85°C;

[0058] 3) Measure 30kg of hydrogenated rosin and 1.4Kg of diisooctyldiphenylamine into the second stirred tank, and mix evenly with 150BS bright stock heated to 80-85°C with stirring;

[0059] 4) Pump the homogeneously mixed product in step 3) to the first stirred tank, then sequentially transport 10kg of anti-diffusion agent, 0.28kg of wetting agent, and 0.03kg of defoamer to the first stirred tank, stir and mix After homogenization, high-temperature rosin active oil is obtained.

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Abstract

High-temperature rosin activated oil and a manufacturing method thereof are provided. The high-temperature rosin activated oil comprises, by weight, 100 parts of 150BS brightening oil, 20-50 parts ofhydrogenated rosin, and 5.5-18.5 parts of functional additives. 20-60% of 159BS brightening oil is metered and pumped into a first stirring kettle; temperature is raised to 40-60 DEG C; the residue ofthe 150BS brightening oil is metered and pumped into a second stirring kettle; the temperature is raised to 89-85 DEG C; hydrogenated rosin and a high-temperature antioxidant are metered and added into the second stirring kettle and are mixed well with the 150BS brightening oil that is stirred and heated to 80-85 DEG C; a uniform mixture is pumped into the first stirring kettle; the functional additives are metered and added sequentially into the first stirring kettle, and high-temperature rosin activated oil is attained after uniform mixing. The high-temperature rosin activated oil and the manufacturing method thereof have the advantages that activity of rosin is significantly improved, anti-spreading and wetting properties are good, wax patterns rarely experience burred edge, resourcesare saved, and production cost is lowered.

Description

technical field [0001] The invention relates to high-temperature rosin active oil and a manufacturing method thereof, and belongs to the technical field of chemical material combination. Background technique [0002] Rosin is an important chemical raw material and a limited natural resource, widely used in all aspects of industry and national economy. At present, the real wax printing and dyeing of the printing and dyeing industry needs to use a large amount of rosin. Under normal circumstances, rosin will become dry and brittle after a real wax printing and dyeing process, lose its activity, and thus lose its use value. [0003] In order to give full play to the use value of rosin and save natural resources, a new technical means is urgently needed to activate the activity of used rosin so that it can be recycled. Contents of the invention [0004] In order to solve the problems in the background technology, the present invention provides a method for manufacturing high...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06B11/00D06P5/12C09F1/02C08J11/04
CPCC08J11/04C09F1/02D06B11/00D06P5/12Y02P20/143Y02W30/62
Inventor 李文婷张立佳李洪强李衍翰
Owner SHANDONG KEYSTONE LUBRICANT TECH