A kind of attapulgite decorative mortar and its preparation method
A technology of facing mortar and attapulgite, which is applied in the field of building materials, can solve the problems of changing decorative effect, unstable coloring, decorative mortar air permeability and loss of decorative style, so as to improve compressive strength and flexural strength, and solve the problem of turtle Crack and micro-crack defects, maintain breathability and decorative style effect
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Embodiment 1
[0035]Preparation of modified epoxy resin:
[0036](1) Put 15 parts of chitosan solid into the reactor, add 5% mass fraction of acetic acid solution to prepare chitosan acetic acid solution for use;
[0037](2) Add 20 parts of epichlorohydrin to the absolute ethanol, heat to reflux, keep stirring for 10 minutes, then add 20 parts of trimethylolethane and 2 parts of benzoyl peroxide, and continue to reflux and stir for 1 hour; Then add the chitosan acetic acid solution in step 1 and 1 part of sodium pyrophosphate, continue to reflux and stir for 2 hours, filter while hot, and wash off impurities with deionized water and absolute ethanol for the precipitation, and send it to a drying oven at 100-110°C for drying To constant weight, the modified epoxy resin is obtained.
[0038]Preparation of modified attapulgite: add 0.3 parts of tripolyphosphoric acid and 0.3 parts of sodium silicate to 75 parts of deionized water, stir until completely dissolved, then add 20 parts of attapulgite, mechanicall...
Embodiment 2
[0043]Preparation of modified epoxy resin:
[0044](1) Put 15 parts of chitosan solid into the reaction kettle, add 5% mass fraction of acetic acid solution to prepare chitosan acetic acid solution for use;
[0045](2) Add 20 parts of epichlorohydrin to the absolute ethanol, heat to reflux, keep stirring for 10 minutes, then add 20 parts of trimethylolethane and 2 parts of benzoyl peroxide, and continue to reflux and stir for 1 hour; Then add the chitosan acetic acid solution in step 1 and 1 part of sodium pyrophosphate, continue to reflux and stir for 2 hours, filter while hot, and wash off impurities with deionized water and absolute ethanol for the precipitation, and send it to a drying oven at 100-110°C for drying To constant weight, the modified epoxy resin is obtained.
[0046]Preparation of modified attapulgite: add 0.3 parts of tripolyphosphoric acid and 0.3 parts of sodium silicate to 75 parts of deionized water, stir until completely dissolved, then add 20 parts of attapulgite, mec...
Embodiment 3
[0064]Based on Example 1, Comparative Example 1 without modification of epoxy resin was set up. Comparative Example 2 without modification of attapulgite was set.
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