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A kind of heat treatment method of diamond composite blank

A heat treatment method and composite material technology, which is applied in the field of diamond composite material production, can solve problems such as inability to clean blanks and performance degradation of diamond composite materials, and achieve the effect of achieving a high degree of cleanliness and meeting production requirements

Active Publication Date: 2020-04-21
BEIJING GANG YAN DIAMOND PROD CO +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The purpose of the present invention is to provide a heat treatment method for a diamond composite material blank, which overcomes the problems in the prior art that the blank cannot be cleaned as a whole and the performance of the diamond composite material produced due to incomplete cleaning of the mixed powder in the blank is reduced. It meets the surface cleaning requirements of the mixed powder in the billet, and can also clean the billet through overall heat treatment. The oxygen content of the mixed powder in the diamond composite billet is reduced to less than 100ppm, and the interface bonding strength is increased by 5%-10%.

Method used

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  • A kind of heat treatment method of diamond composite blank
  • A kind of heat treatment method of diamond composite blank
  • A kind of heat treatment method of diamond composite blank

Examples

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Effect test

Embodiment 1

[0031] A heat treatment method for a diamond composite material blank, comprising the following steps:

[0032] 1) will follow figure 1 The assembled diamond composite material blank (size specification Φ1613mm) is placed in the vacuum furnace, and a batch of 200 diamond composite material blanks are placed in the same vacuum furnace;

[0033] 2) Vacuum the furnace so that the air pressure in the furnace reaches 7.5*10 -3 Below Pa, start to heat up slowly, heat from room temperature to 150°C in 30 minutes, and keep it warm for half an hour; then continue to vacuumize and heat up, and raise the temperature to 550°C in 1.5 hours, while the pressure in the furnace is stable at 4*10 -3 Below Pa;

[0034] 3) The temperature in the furnace is kept at 550°C for 1 hour, and at the same time, the vacuum furnace is intermittently filled with hydrogen and vacuumized, and the whole billet is degassed and reduced for heat treatment: first, a certain amount of hydrogen is charged into the...

Embodiment 2

[0038] A heat treatment method for a diamond composite material blank, comprising the following steps:

[0039] 1) will follow figure 1 The assembled diamond composite material blank (size specification Φ1913mm, 100 pieces) is placed in the vacuum furnace;

[0040] 2) Vacuum the furnace so that the air pressure in the furnace reaches 7*10 -3 Below Pa, start to heat up slowly, heat from room temperature to 150°C in 30 minutes, and keep it warm for half an hour; then continue to vacuumize and heat up, and raise the temperature to 580°C in 1.5 hours, while the pressure in the furnace is stable at 3*10 -3 Below Pa;

[0041] 3) The temperature in the furnace is kept at 580°C for 1 hour, while the vacuum furnace is intermittently filled with hydrogen and vacuumized, and the whole billet is degassed and reduced for heat treatment: first, a certain amount of hydrogen is charged into the vacuum furnace, and then The amount of hydrogen into the furnace makes the pressure in the furna...

Embodiment 3

[0045] A heat treatment method for a diamond composite material blank, comprising the following steps:

[0046] 1) will follow figure 1 The assembled diamond composite material blanks (size specification Φ1313mm, 400 pieces) are placed in the vacuum furnace;

[0047] 2) Vacuum the furnace so that the air pressure in the furnace reaches 6.5*10 -3 Below Pa, start to heat up slowly, heat from room temperature to 150°C (ie the first temperature) in 30 minutes, and keep it warm for half an hour; then continue to vacuumize and heat up, and heat up to 600°C (ie the second temperature) in 1.5 hours, At the same time, the air pressure in the furnace is stable at 3*10 -3 Below Pa;

[0048] 3) The temperature in the furnace is kept at 600°C for 1.5 hours, while the vacuum furnace is intermittently filled with hydrogen and vacuumized, and the whole billet is degassed and reduced for heat treatment: first, a certain amount of hydrogen is charged into the vacuum furnace, and the vacuum f...

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Abstract

The invention discloses a heat treatment method of a diamond composite material blank. The heat treatment method sequentially comprises the following steps that step 1, the assembled diamond compositematerial blank is placed into a vacuum hearth, and after heating is carried out to a first temperature under a vacuum condition, heat is preserved for a certain time; step 2, the blank obtained in the step 1 is continuously heated to a second temperature under the vacuum condition, heat is preserved for a certain time, and intermittent hydrogen charging and vacuumizing treatment are carried out on a vacuum furnace while the heat is preserved; and step 3, the blank obtained in the step 2 is cooled to a third temperature under the vacuum condition, filling of inert gas or nitrogen is carried out until normal pressure is reached, and the blank is continuously cooled to normal temperature. Compared with an existing purification vacuum treatment method, the oxygen content of the mixed powder in the diamond composite material blank is reduced less than 100 ppm from 600 ppm, the interface bonding strength of produced diamond composite material samples is improved by 5-10%, and the high cleanliness of the whole diamond composite material blank is realized.

Description

technical field [0001] The invention belongs to the technical field of diamond composite material production, and in particular relates to a heat treatment method for a diamond composite material blank, which is used for pre-heat treatment and purification of the diamond composite material blank before high temperature and high pressure synthesis. Background technique [0002] During the high-pressure and high-temperature synthesis of diamond composite materials, the adsorption of gas and impurities on the surface of diamond micropowder particles in the mixed powder of diamond composite material blanks, as well as the purity and oxidation of the binder will directly affect the performance of diamond composite materials. The diamond micropowder used in diamond composite materials is a fine particle powder obtained by mechanical crushing of diamond single crystal particles. Its surface is rough and shaped in various shapes, with large surface area and high specific surface ener...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C22C26/00C22C1/05C22C1/10B22F7/04B22F3/10
CPCB22F3/1017B22F7/04B22F2007/042C22C1/05C22C26/00
Inventor 孙延龙刘一波尹翔陈建立徐燕军徐良
Owner BEIJING GANG YAN DIAMOND PROD CO