Aluminum hydroxide with low oil absorption value and its preparation method and application
A technology of aluminum hydroxide and activated aluminum hydroxide, which is applied in the preparation of alkali metal aluminate/alumina/aluminum hydroxide, can solve problems such as high oil absorption value, reduced flame retardancy, and poor filling performance, and achieves Reduce oil absorption value, improve flame retardant effect, increase the effect of filling amount
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[0016] The first aspect of the present invention provides a method for preparing aluminum hydroxide with low oil absorption value, wherein the method comprises the following steps:
[0017] (1) adding an organic compound containing polyhydroxyl groups to the Bayer process sodium aluminate solution and mixing uniformly to obtain a raw material solution;
[0018] (2) carrying out the first division of the raw material liquid and the activated aluminum hydroxide seed slurry to obtain a decomposition liquid;
[0019] (3) performing a second separation of the decomposed liquid and an organic acid insoluble in the decomposed liquid to obtain a decomposed slurry;
[0020] (4) Rapidly raising the temperature of the decomposed slurry for crystallization, then removing the organic acid salt, and filtering, washing and drying the obtained slurry to obtain aluminum hydroxide with low oil absorption value.
[0021] In the present invention, the preparation method of the Bayer process sodi...
preparation example 1
[0042] Preparation of active aluminum hydroxide seed slurry 1: Mix 50g of aluminum hydroxide fine powder (particle size: 62 μm, purchased from Luoyang Xiangjiang Wanji Aluminum Co., Ltd., batch: 20161220) with 1L of deionized water, with a solid content of 50g / L, using a ball mill (purchased from Foshan Yejin Electromechanical Equipment Co., Ltd., the model is YJKS) to grind the aluminum hydroxide particles in the above mixture to the median particle size (D 50 )=0.6-1.0 μm, the obtained aluminum hydroxide slurry is the active aluminum hydroxide seed slurry.
preparation example 2
[0044] Preparation of active aluminum hydroxide seed slurry 2: Mix 200g of aluminum hydroxide fine powder with 1L of deionized water, with a solid content of 200g / L, and use a ball mill to grind the aluminum hydroxide particles in the above mixture to D 50 =0.6-1.0 μm, the obtained aluminum hydroxide slurry is the activated aluminum hydroxide seed slurry.
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Abstract
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