Rigid foam plastic and preparation method thereof
A technology for rigid foam plastics and raw materials, applied in the field of packaging materials, can solve the problems of low tensile strength and low compressive strength, and achieve the effects of simple raw materials, easy availability of raw materials, and simple preparation methods
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Embodiment 1
[0024] Step 1: Weigh 100 parts of polymethylene polyphenylisocyanate, 10 parts of polydimethylsiloxane, 60 parts of polyether, 0.1 part of catalyst, 4 parts of triethylenediamine, TCEP 40 parts, 2 parts of distilled water, 5 parts of fluorodichloroethane, 1 part of dimethylcyclohexylamine, and 0.5 parts of hexahydrotriazine.
[0025] Step 2: Put all raw materials into a high-speed mixer and mix evenly. The temperature of the mixer is 20°C, the mixing speed is 1000r / min, and the mixture is mixed for 10s.
[0026] The third step: put the mixed material into the mold, the mold temperature is 40°C, the curing temperature is 90°C, and rises for 110s.
[0027] Product density is 0.034g / cm3, tensile strength is 250MPa, compression deformation is 5.5%; compressive strength is 240MPa, thermal conductivity is 0.02W / (m K); product bonding strength is 310MPa, raw materials are easy to obtain, preparation method is simple, elongation Rate 140%.
Embodiment 2
[0029] Step 1: Weigh 100 parts of polymethylene polyphenylisocyanate, 20 parts of polydimethylsiloxane, 70 parts of polyether, 0.5 parts of catalyst, 8 parts of triethylenediamine, TCEP 60 parts of distilled water, 25 parts of fluorodichloroethane, 5 parts of dimethylcyclohexylamine, and 4.5 parts of hexahydrotriazine.
[0030] Step 2: Put all the raw materials into a high-speed mixer and mix evenly. The temperature of the mixer is 30°C, the mixing speed is 1400r / min, and the mixing is 20s.
[0031] Step 3: The mixed material is put into the mold, the mold temperature is 45°C, the curing temperature is 100°C, and rises for 130s.
[0032] Product density 0.035g / cm3, tensile strength 260MPa, compression deformation 5%; compressive strength 250MPa, thermal conductivity 0.021W / (m K); product bonding strength 320MPa, raw materials are simple and easy to obtain, simple preparation method, elongation Rate 150%.
Embodiment 3
[0034] Step 1: Weigh 100 parts of polymethylene polyphenylisocyanate, 10 parts of silicone oil, 65 parts of polyether, 0.2 parts of catalyst, 5 parts of triethylenediamine, 45 parts of TCEP, and 3 parts of distilled water according to the ratio of parts by mass. 10 parts of fluorodichloroethane, 2 parts of dimethylcyclohexylamine, and 1.5 parts of hexahydrotriazine.
[0035] Step 2: Put all raw materials into a high-speed mixer and mix evenly. The temperature of the mixer is 20°C, the mixing speed is 1000r / min, and the mixture is mixed for 10s.
[0036] The third step: put the mixed material into the mold, the mold temperature is 40°C, the curing temperature is 90°C, and rises for 110s.
[0037] Product density is 0.036g / cm3, tensile strength is 270MPa, compression deformation is 4.5%; compressive strength is 260MPa, thermal conductivity is 0.022W / (m K); product bonding strength is 330MPa, raw materials are easy to obtain, preparation method is simple, elongation Rate 160%. ...
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Abstract
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