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Jasmine essence for blasting bead for cigarette and preparation method and application of jasmine essence

A jasmine essence and jasmine technology, applied in the field of flavors and fragrances, to achieve the effect of improving comfort and reducing irritation

Inactive Publication Date: 2019-04-12
CHINA TOBACCO HENAN IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

But the cigarette with jasmine fragrance has not been reported yet, and all the essences used in the above patents are formulated with extracts, absolutes and synthetic spices

Method used

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  • Jasmine essence for blasting bead for cigarette and preparation method and application of jasmine essence
  • Jasmine essence for blasting bead for cigarette and preparation method and application of jasmine essence
  • Jasmine essence for blasting bead for cigarette and preparation method and application of jasmine essence

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] A method for separating and preparing jasmine characteristic components, the steps are as follows:

[0026] (1) Weigh 120 g of silica gel into a 500 mL beaker, add a mixed solvent of petroleum ether and ethyl acetate with a volume ratio of 12:1, stir well, and then pour it into a Φ2.1 cm×70 cm separation column at one time, and repeat. Rinse to make the silicone evenly compact;

[0027] (2) Weigh 0.6 g of jasmine extract into a 50 mL eggplant-shaped bottle, add 2 mL of ethyl acetate to dissolve and dilute, and then use a disposable dropper to slowly and evenly spread the diluted jasmine extract on the silica surface;

[0028] (3) Control the flow rate of the eluent to be 3mL / min with a DHL-N computer digital display timing constant flow pump, and elute according to the volume ratio of petroleum ether and ethyl acetate as a gradient of 12-4:1, each gradient elution The volume of the reagent is 400 mL, and the eluate is collected in separate tubes with a DBS-40 computer ...

Embodiment 2

[0036] The characteristic fragrance components of jasmine prepared in Example 1, benzyl acetate, methyl jasmonate, jasmine lactone, nerolidol, linalool, jasmonone, and benzyl alcohol, are configured into jasmine essence according to mass percentage, Its proportions are as follows:

[0037] 20% benzyl acetate, 10% methyl jasmonate, 16% jasmonolide, 6% nerolidol, 20% linalool, 20% jasmonone, 8% benzyl alcohol.

[0038] The jasmine essential oil and glyceryl caprylic acid were prepared according to the mass ratio of 10:90 to obtain the cigarette popping beads with jasmine fragrance characteristics, and the diameter of the popping beads was 2 mm. The essence content in the popped beads is 22 μL / grain.

Embodiment 3

[0040]The characteristic aroma components of jasmine extract prepared in Example 1 are benzyl acetate, methyl jasmonate, jasmonolactone, nerolidol, linalool, jasmone, and benzyl alcohol, and are configured into jasmine Fragrance, in proportions as follows:

[0041] 12% Benzyl Acetate, 8% Methyl Jasmonate, 20% Jasmonolactone, 4% Nerolidol, 24% Linalool, 20% Jasmone, 12% Benzyl Alcohol.

[0042] The jasmine essential oil and caprylic acid glycerin were prepared according to the mass ratio of 12:88 to obtain the cigarette popping beads with the characteristic aroma of jasmine, and the diameter of the popping beads was 2.8 mm. The essence content in the popping beads is 25 μL / capsule.

[0043] According to the existing filter rod production process, the popping beads are put into the center of the filter rod through the filter rod forming machine, and added to the ordinary circumference (24.3mm) cigarette filter rod. Popping beads, that is, the popping beads filter stick, and af...

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Abstract

The invention discloses jasmine essence for a blasting bead for a cigarette and a preparation method and application of the jasmine essence. The jasmine essence is prepared from, by mass, 10-20% of benzyl acetate, 2-10% of jasmonic acid methyl ester, 10-20% of Jasmine lactone, 3-6% of nerolidol, 15-25% of linalool, 10-20% of jasmine and 10-15% of benzyl alcohol. The cigarette with jasmine flower fragrance is prepared, raw materials required for preparing the jasmine essence are separated from extract of natural jasmine products and obtained, and the defect that synthetic essence only has the shape same with a natural perfume material and no essence of the natural perfume material is overcome. Through separation of a column chromatography technology, the mixed odor influence of jasmine extract and macromolecule substances of pectin, protein, fiber and the like in the essence on the sensory quality of the cigarette is reduced. The prepared blasting bead can reduce stimulation of the cigarette, mixed odor of the cigarette is reduced, the comfort degree of the cigarette is improved, and the cigarette has the jasmine fragrance characteristic.

Description

technical field [0001] The invention belongs to the field of flavors and fragrances, and in particular relates to a jasmine flavor for cigarette popping beads, a preparation method and application thereof. Background technique [0002] Jasmine ( Jasminum sambac ) is an evergreen shrub or vine of the Oleaceae family. From ancient times to the present, jasmine has been loved by people because of its elegant and fragrant aroma. The jasmine essential oil, extract and other spices extracted from jasmine are widely used in the flavor and fragrance industry. On the one hand, as a spice, it can be used to make perfumes for daily use, especially when making high-end perfumes, the aroma of jasmine is an essential ingredient, and there is even a saying that "without jasmine, there is no perfume". Jasmine spice can also be used to make edible flavors used in food, especially for dessert wines, condiments, and flavors for baked goods. [0003] The traditional flavoring technology is to...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11B9/00A24B15/30
CPCA24B15/301A24B15/302C11B9/0003C11B9/0061
Inventor 郭华诚李阳光郜海民张峻松尹献忠吴艳艳张爱忠高尊华许淑红张月华王颖张健王军罗华丽杨耀伟张文海宋六明
Owner CHINA TOBACCO HENAN IND
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