Urethane resins for polyurethane adhesives
A technology of alkyl carbamate and polyurethane, applied in the field of carbamate resin for polyurethane adhesive, can solve problems such as difficulty in high bonding strength
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[0071] Preparation of modified cured rubber layer
[0072] The following components were mixed in the proportions given in Table 1 and mixed at room temperature for a sufficient period of time to obtain an uncured rubber compound.
[0073] Table 1: Uncured Rubber Compositions
[0074]
[0075]The uncured rubber compound was then divided into 4 batches. A 1:0.3 molar ratio of butyl carbamate:formaldehyde mixture was then added to 3 of the 4 batches of uncured rubber compound in amounts of 2phr, 5phr and 10phr respectively, the last batch of uncured rubber compound containing no Butyl carbamate: formaldehyde mixture. Each batch was individually cured at 145°C for 33 minutes at 100 psi. The resulting cured rubber compound was then prepared for adhesion by polishing the bonding surface. Surface polishing with a handheld orbital sander is continued for a sufficient period of time until the surface is visibly altered by sanding. The bonding surface of the polyurethane subs...
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