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A kind of preparation method of multifunctional colored real silk or wool fabric

A multi-functional, fabric technology, applied in textiles and papermaking, animal fibers, fiber processing, etc., can solve the problems of poor water repellency and anti-ultraviolet performance, low water repellency and flame retardant performance of silk, poor functional finishing effect, etc. The effect of good promotion value, low equipment requirements, and simple and easy preparation method

Active Publication Date: 2021-12-14
SUZHOU UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Silk and wool have better comfort and warmth retention properties, and are ideal fabrics for outdoor clothing, but their water repellency and UV resistance are not good, so they need to be functionally finished
The prior art discloses a colored flame-retardant and water-repellent real silk fabric and a preparation method thereof, including the following steps: (1) soaking the real silk fabric in an aqueous solution of dopamine for shaking treatment, then taking it out for washing and drying to obtain a colored fabric containing polydopamine; real silk fabric; (2) immerse the colored real silk fabric obtained in step (1) in the fluorozirconate aqueous solution, make the polydopamine on the colored real silk fabric react with fluorozirconate, then take out cold water and rinse and dry to obtain colored Flame-retardant and water-repellent silk fabrics; the prior art also discloses a preparation method of a multifunctional silk-containing fabric, first using dopamine aqueous solution to impregnate the silk-containing fabric, then using a reducing agent to impregnate it, and finally using a metal compound solution to The fabric treated with the reducing agent is dipped and finished to make a multifunctional silk-containing fabric. The LOI value of the finally obtained multifunctional silk-containing fabric is ≥29.1%, its UPF value is ≥10.79, and its contact angle is ≥128.5°. However, it is more cumbersome, and the water-repellent and flame-retardant performance of the obtained silk is relatively low, and the functional finishing effect is poor.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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  • A kind of preparation method of multifunctional colored real silk or wool fabric
  • A kind of preparation method of multifunctional colored real silk or wool fabric
  • A kind of preparation method of multifunctional colored real silk or wool fabric

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0034] A preparation method of a multifunctional colored silk fabric, the steps are as follows:

[0035] (1) Cleaning and drying silk fabrics: first use soap solution with a temperature of 40°C and a concentration of 4g / L to wash for 30 minutes, then use clean water to wash 4 times, and finally dry at a temperature of 80°C for 20 hours to obtain the washing and drying fabric. After the silk fabric;

[0036] (2) Functional finishing: Weigh ferric chloride hexahydrate into a three-necked flask, add deionized water to dissolve it, and put it into the washed and dried silk fabric for dipping. The dipping temperature is 75°C, and the dipping time is 1h. The ratio is 1:50, Fe in the impregnation solution 3+ The concentration is 0.03mol / g;

[0037] (3) After finishing, take out the real silk fabric and dry it at 80° C. for 12 hours.

[0038] Such as image 3 and 4 As shown, the superhydrophobic contact angle of the multifunctional colored silk fabric is 163.5°, which is much hig...

Embodiment 2

[0050] A preparation method of a multifunctional colored wool fabric, the steps are as follows:

[0051] (1) Washing and drying wool fabrics: first use soap solution with a temperature of 40°C and a concentration of 4g / L to wash for 30 minutes, then use clean water to wash 4 times, and finally dry at a temperature of 80°C for 20 hours to obtain the washing and drying fabric. After the wool fabric;

[0052] (2) Functional finishing: Weigh ferric chloride hexahydrate into a three-necked flask, add deionized water to dissolve it, and put it into the washed and dried wool fabric for immersion. The immersion temperature is 75°C, and the immersion time is 1h. The ratio is 1:50, Fe in the impregnation solution 3+ The concentration is 0.03mol / g;

[0053] (3) After finishing, take out the wool fabric and dry it at 80°C for 12 hours.

[0054] Such as Figure 5 As shown, the superhydrophobic contact angle of the multifunctional colored wool fabric is 159.4°, and the hydrophobic effec...

Embodiment 3

[0057] A preparation method of a multifunctional colored silk fabric, the steps are as follows:

[0058] (1) Cleaning and drying silk fabrics: first use soap solution with a temperature of 30°C and a concentration of 2g / L to wash for 40 minutes, then use clean water to wash 5 times, and finally dry at a temperature of 80°C for 24 hours to obtain a cleaning and drying fabric. After the silk fabric;

[0059] (2) Functional finishing: Weigh ferric chloride hexahydrate into a three-necked flask, add deionized water to dissolve it, and put it into the washed and dried silk fabric for dipping. The dipping temperature is 70°C, and the dipping time is 2 hours. The ratio is 1:50, Fe in the impregnation solution 3+ The concentration is 0.032mol / g;

[0060] (3) After finishing, take out the real silk fabric and dry it at 80°C for 24 hours.

[0061] The superhydrophobic contact angle of the multifunctional colored silk fabric is 163.7°, the LOI of the multifunctional colored silk fabri...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Abstract

The present invention relates to a kind of preparation method of multifunctional colored real silk or woolen fabric, adopts Fe-containing 3+ The solution is used to finish silk or wool fabrics to make multifunctional colored silk or wool fabrics, wherein the finishing method is dipping, and the finishing temperature is 70-80°C. The superhydrophobic contact angle of the prepared multifunctional colored silk fabric is ≥163.5°, the LOI is ≥36.6%, the UPF value is ≥17.56, the UVA value is ≤6.70%, and the UVB value is ≤6.80%; the superhydrophobic contact angle of the multifunctional colored wool fabric is ≥ 159.4°, the LOI of multifunctional colored wool fabric is ≥32.5%, the UPF value is ≥236.16, the UVA value is ≤0.70%, and the UVB value is ≤0.74%. The inventive method is by depositing a large amount of Fe at real silk or wool fabric 3+ , significantly improved its flame retardant performance, hydrophobic performance and anti-ultraviolet performance, and the functional finishing effect is good.

Description

technical field [0001] The invention belongs to the technical field of textile functional finishing, and relates to a preparation method of multifunctional colored silk or wool fabric. Background technique [0002] As a kind of natural fiber, real silk fabric has excellent comfort, soft luster and soft feel, and has excellent moisture absorption and breathability and health care performance, etc., and is widely used in the preparation of interior decoration products such as curtains and lighting decorations. Wool is a natural high polymer containing protein. Because of its good hygroscopicity, heat preservation and comfort, it is widely used in clothing, construction and home textiles and other fields. [0003] Silk and wool have high nitrogen content, which endows them with certain flame retardancy, but with the wide application of silk and wool in various fields, its natural flame retardancy has become more and more difficult to meet people's needs, especially It is the a...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D06M11/28D06M101/12D06M101/10
CPCD06M11/28D06M2101/12D06M2101/10
Inventor 关晋平宣凯陈国强唐人成
Owner SUZHOU UNIV
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