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Water volatile oil distilling and extracting device and method

A technology of water distillation and volatile oil, which is applied in the direction of essential oil/fragrance, fat production, etc., can solve the problem of incomplete condensation, achieve high cooling efficiency, improve oil-water separation efficiency, and reduce the possibility

Inactive Publication Date: 2019-08-06
QIQIHAR UNIVERSITY
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  • Application Information

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Problems solved by technology

The water distillation method can reduce the loss of volatile oil in the distillation process, but in the methods reported in the existing literature, there is a lack of a better laboratory device for the extraction of volatile oil by the water distillation method
Therefore, it is necessary to invent a device and method for extracting volatile oil by distillation in water, overcome the disadvantages of distillation in water and solve problems such as incomplete condensation, and improve the extraction efficiency, extraction rate and quality of volatile oil

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  • Water volatile oil distilling and extracting device and method
  • Water volatile oil distilling and extracting device and method
  • Water volatile oil distilling and extracting device and method

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Embodiment Construction

[0018] The device for extracting volatile oil by distillation on water and the method for extracting volatile oil with the device will be further described below.

[0019] The above-water distillation extracting volatile oil device described in the present invention has a structure such as figure 1 , figure 2 , image 3 As shown, it includes a round bottom flask 1, a steaming tube 3, and a closed and condensed integrated volatile oil extractor (4-14); , separation collection pipe 10, scale pipe 12, return branch pipe 13, cock 14; Described spherical condenser pipe 7 is provided with water inlet 11 and water outlet 6; Described tool plug branch pipe 8 comprises branch pipe hollow plug 15 and ventilation branch pipe 16 ( Both are 5# standard grinding mouth), the branch pipe hollow plug 15 is a bottomless hollow plug, the branch pipe hollow plug 15 and the side wall of the ventilation branch pipe 16 have ventilation holes 17 corresponding to each other, and the diameter of the...

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Abstract

The invention discloses a water volatile oil distilling and extracting device and method. Compared with conventional distillation extraction methods, both the extraction rate and sensory quality of volatile oil can be enhanced, and the extraction rate can be enhanced by 3-4 times. The device is characterized in that the device includes a round bottom flask, a material steaming pipe and an enclosing and condensation integrated volatile oil extractor; water is put in the flask, and a material is put in the material steaming pipe; water vapor passes through the material and carries volatile oil;condensation is performed in an Allihn condenser from top to bottom; oil and water separation is performed in a separating and collecting pipe under a low temperature environment to perform full cooling; and the precision of a scale pipe reaches 0.01 mL, so that the volume of the volatile oil can be read more accurately. Therefore, the vacancy problem of water volatile oil distilling and extracting devices in laboratories can be solved; the problems of hydrolysis and pyrolysis of volatile oil components caused by long-time soaking of the materials in boiling water can be solved; enclosed condensation and cooling systems can prevent the natural dissipation of the volatile oil during extraction; and accurate scales provide reliable data for the scientific research of the laboratories.

Description

technical field [0001] The invention belongs to the technical field of volatile oil extraction, and in particular relates to a device for extracting volatile oil by distillation over water, and a method for extracting volatile oil by distillation over water using the device. Background technique [0002] Volatile oils, also known as essential oils and aromatic oils, are secondary metabolites of plants, widely present in the whole plant, and distributed unevenly in plant organs such as branches, leaves, bark, trunks, roots, flowers, fruits, and seeds. Under normal circumstances, volatile oils are oily liquids, and a few are solid; volatile oils are volatile, refracting and optically active; easily soluble in organic solvents such as petroleum ether and ethanol, but insoluble in water; most volatile oils are lighter than water, and a few heavier than water. Volatile oil is a complex mixture, generally containing several to dozens or hundreds of different components, most of w...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11B9/02
CPCC11B9/027
Inventor 刘红霞王大元仝锦豪武露丁荣良董璐元田云阔李天爱
Owner QIQIHAR UNIVERSITY
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