A fast-curing silicone sealant
A fast-curing, silicone-based technology, applied in the direction of adhesives, non-polymer adhesive additives, adhesive additives, etc., can solve the problems of high metering accuracy, inability to increase curing speed, and slow curing speed
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Embodiment 1
[0028] A condensation-type fast-curing silicone sealant, including A and B components. Component A includes 100 parts of α, ω-dihydroxy polydimethylsiloxane (viscosity 36000mPa·s), 50 parts of monohydroxyl-terminated simethicone oil (0.6% volatile content), 15 parts of dimethyl silicone oil, Calcium carbonate and white carbon black mixture (10:1) 60 parts, glycerin 5 parts, methyltrimethoxysilane 0.3 parts, dibutyltin dilaurate 0.5 parts; B component includes simethicone oil 45 parts, 5 parts of N-aminoethylpiperazine, 1.5 parts of tetrabutylammonium bromide, 20 parts of amino silicone oil, 0.2 part of methyltrimethoxysilane, said amino silicone oil is octamethylcyclotetrasiloxane and N-( β-Aminoethyl)-γ-aminopropylmethyldimethoxysilane (HD103) is prepared by mixing at a mass ratio of 1:1 and reacting at 110-120°C.
[0029] The preparation of component A includes the following two steps:
[0030] (1) Calcium carbonate, white carbon black and methyltrimethoxysilane are weighe...
Embodiment 2
[0036] A condensation-type fast-curing silicone sealant, including A and B components. Component A includes 100 parts of α, ω-dihydroxy polydimethylsiloxane (viscosity 25000mPa·s), 50 parts of monohydroxyl-terminated dimethyl silicone oil (0.6% volatile content), 18 parts of dimethyl silicone oil, Calcium carbonate and white carbon black mixture (12:1) 60 parts, ethylene glycol 5 parts, methyltrimethoxysilane 0.3 part, dibutyltin dilaurate 0.5 part; B component and preparation method are the same as the examples 1.
Embodiment 3
[0038] A condensation-type fast-curing silicone sealant, including A and B components. Component A includes 100 parts of α, ω-dihydroxy polydimethylsiloxane (viscosity 25000mPa·s), 50 parts of monohydroxyl-terminated dimethyl silicone oil (0.7% volatile content), 15 parts of dimethyl silicone oil, Calcium carbonate and white carbon black mixture (12:1) 60 parts, glycerol 5 parts, dimethyldimethoxysilane 3 parts, dibutoxydihexyltin 2 parts; B component includes dimethyl 40 parts of silicone oil, 5 parts of N-aminoethylpiperazine, 2 parts of tetraethylammonium bromide, 20 parts of amino silicone oil, 0.2 part of methyltrimethoxysilane, the amino silicone oil is octamethylcyclotetrasiloxane It is prepared by mixing with N-(β-aminoethyl)-γ-aminopropylmethyldimethoxysilane (HD103) at a mass ratio of 1:1 and reacting at 110-120°C.
[0039] The preparation method of A and B components is the same as in Example 1.
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Abstract
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