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Low carbonyl value soybean oil preparation method

A technology of soybean oil and carbonyl value, which is applied in the direction of fat oil/fat refining and fat production, and can solve the problem of high carbonyl value

Active Publication Date: 2019-10-22
SOUTHSEAS OILS & FATS INDAL CHIWAN
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] In view of the above-mentioned deficiencies in the prior art, the purpose of the present invention is to provide a method for preparing soybean oil with low carbonyl value, aiming at solving the problem of high carbonyl value of refined soybean oil under the existing technology

Method used

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preparation example Construction

[0026] A kind of preparation method of low carbonyl value soybean oil provided by the present invention, described method specifically comprises the steps:

[0027] S100, passing the pretreated soybean oil into the first container, and adding the adsorbent into the first container under vacuum conditions to obtain a mixture;

[0028] Specifically, please refer to figure 1 After the soybean oil is desoaped, it is passed into a drying tank and dried under vacuum conditions. The dried soybean oil is put into a pre-decolorization reaction tank, and the soybean oil is heated to 70-120°C under vacuum conditions. Add the adsorbent under stirring condition, stir to obtain the mixture of soybean oil and adsorbent, and wait for filtration. The vacuum condition is that the degree of vacuum is less than -680mmHg.

[0029] In some embodiments, the adsorbent includes activated clay and / or activated carbon. In terms of mass percentage, the added amount of the adsorbent accounts for 0.5%-7...

Embodiment 1

[0043] Soybean oil after chemical alkali refining is put into the pre-bleaching reaction tank after vacuum drying at 70°C. Add 4.5% activated clay at 110°C and the system vacuum is -720mmHg, and flow into the decolorization tank for 30 minutes. This process is accompanied by direct steam stirring, and the decolorization is completed. After filtering through the filter, the filter sheet needs to be pre-coated before filtering. Diatomaceous earth or perlite is mixed with the oil in the pre-coating tank and then circulated through the filter until the oil is clear and transparent after passing through the filter. After the pre-coating is completed After filtering, there will be a small amount of residual oil in the clay filter cake that needs to be blown out with steam. This part of the oil is more seriously oxidized and concentrated and purged to the residual oil tank as ordinary soybean oil. The oil after decolorization and filtration is in the The deodorization temperature is d...

Embodiment 2

[0045]Soybean oil that has undergone chemical alkali refining is vacuum-dried at 80°C and put into the pre-decolorization reaction tank. At 85°C and the system vacuum is -720mmHg, add 1.0% bleaching clay and 0.5% activated carbon into the decolorization tank for 30 minutes. The process is accompanied by Stir directly with steam, and filter through a filter after decolorization is completed. Before filtering, the filter sheet needs to be pre-coated. Diatomaceous earth or perlite is mixed with the oil in the pre-coating tank and then circulated through the filter until the oil is clear after passing through the filter. Transparent, after the pre-coating is completed, filter. After filtering, there will be a small amount of residual oil in the clay filter cake that needs to be blown out with steam. This part of the oil is more oxidized and concentrated and purged to the residual oil tank as ordinary soybean oil. The grease after decolorization and filtration was directly steam str...

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Abstract

The invention relates to a low carbonyl value soybean oil preparation method, which comprises: introducing pretreated soybean oil into a first container, adding an adsorbent to the first container under vacuum, and mixing to obtain a mixture; introducing the mixture into a second reaction container, and decolorizing under vacuum to obtain a crude soybean oil; and filtering the crude soybean oil under vacuum to obtain a low carbonyl value soybean oil. According to the present invention, by selecting the suitable adsorbent, the soybean oil is adsorbed and decolorized by combining active white clay and active carbon; the adding amount of the adsorbent and the decolorizing temperature are controlled, the original decolorizing filtering system is changed, the pre-coating tank is changed into the vacuum so as to reduce the contact of the soybean oil and the air, and the steam purging soybean oil after filtration is subjected to centralized treatment as the common bean oil; and the carbonyl value in the refined soybean oil obtained by the synergy is less than 6.0 meq / kg, such that the requirements of soybean oil on the carbonyl value in health care medical oil are met.

Description

technical field [0001] The invention relates to the technical field of soybean oil refining, in particular to a method for preparing soybean oil with low carbonyl value. Background technique [0002] During the production and processing of soybean oil, there will be impurities. In order to remove the impurities, soybean oil needs to be refined. [0003] The conventional refining process mostly uses vacuum in the decolorization tank, but the pre-coating tank with filter aid is in a normal pressure state, and after the oil is filtered, the steam purges the filter cake and returns it to the decolorization tank or deodorizes directly after filtration, which makes it difficult to reduce the large amount of oil in the oil refining process. The carbonyl value of soybean oil may lead to its increase, wherein the carbonyl value (carbonyl group value, CGV) refers to the total amount of fatty acids or glycerides containing aldehyde groups and ketone groups and their polymers produced w...

Claims

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Application Information

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IPC IPC(8): C11B3/00C11B3/10C11B3/14
CPCC11B3/001C11B3/008C11B3/10C11B3/14
Inventor 陈云波范艳梅闫红勋朱神通李恒飞
Owner SOUTHSEAS OILS & FATS INDAL CHIWAN