Catalytic reaction equipment and method
A catalytic reaction and equipment technology, applied in chemical instruments and methods, catalytic cracking, cracking, etc., can solve problems such as difficulty in realizing industrialization, the pressure difference between the lifting section and the riser reactor cannot be too large, and the line speed of the lifting regenerant is low. , to reduce side reactions, shorten the oil contact mixing time, and improve the oil contact efficiency.
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Embodiment 1-1
[0124] Example 1-1 is in Figure 1A to Figure 1D The catalyst is MLC-500 produced by Sinopec Qilu Catalyst Factory, and its properties are listed in Table 1.
[0125] Take Daqing wax oil feed rate of 10 kg / hour as an example, the circulation rate of catalyst is 60 kg / hour, the flow rate of water vapor is 600 g / hour, the feed temperature of raw oil is 300℃, the sedimentation The operating pressure for the top and regenerator top is 150 kPa (gauge).
[0126] Such as Figure 1A As shown, the regeneration air 48 enters from the bottom of the regenerator 10 to contact with the catalyst to be burnt and regenerated, and the charred regenerant is drawn from the inclined pipe 11 drawn from the bottom of the regenerator 10 to enter the regenerant stripping agent through the pneumatic switch valve 12 13, the stripping steam 32 continuously enters the regenerant stripper 13 to blow off flue gas and oxygen to the regenerator 10, and the regenerant that basically blows off oxygen is drawn ...
Embodiment 2-1
[0136] This embodiment is carried out with the catalytic cracking operation mode of prolific liquid product, take Daqing wax oil feed rate as the medium-sized device of 60 kg / hour as example, the circulation rate of catalyst is 360 kg / hour, the feed temperature of raw material is 300 °C, the operating pressure at the top of the settler and the top of the regenerator is 150 kPa (gauge pressure), and the outlet temperature of the riser reactor is 495 °C. The properties of Daqing wax oil raw materials are listed in Table 2, and the catalyst is MLC-500 produced by Sinopec Qilu Catalyst Factory, and the properties are listed in Table 1. The specific reaction conditions of this embodiment are shown in Table 2-1, and the specific reaction results are shown in Table 2-2.
[0137]As shown in Figure 1, the temperature of the regenerated agent that is regenerated in the coking section 510 of the regenerator of the catalytic cracking unit is 680 ° C, and enters the regenerated agent strip...
Embodiment 2-2
[0140] This embodiment is carried out with the catalytic cracking operation mode of low-carbon olefin products. Taking Daqing wax oil feed rate as a medium-sized device of 60 kg / hour as an example, the circulation rate of the catalyst is 720 kg / hour, and the catalyst-oil ratio of the reaction is 12 , the feed temperature of the raw material is 280°C, the operating pressure of the settler top and the regenerator top is 150 kPa (gauge pressure), and the outlet temperature of the riser reactor is 560°C. The properties of Daqing wax oil raw materials are listed in Table 2, and the catalyst is CRP-1 produced by Sinopec Qilu Catalyst Factory, and the properties are listed in Table 1. The specific reaction conditions of this embodiment are shown in Table 2-1, the specific reaction results are shown in Table 2-2, and the properties of gasoline products are shown in Table 2-3.
[0141] As shown in Figure 1, the temperature of the regenerated agent after completion of regeneration in th...
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