Benzothiazole derivative, preparation method thereof and application of benzothiazole derivative in rapid visual identification of Baijiu alcoholic strength
A technology of benzothiazole and derivatives, applied in the field of fluorescent materials, can solve the problems of unintuitive measurement results, complicated sample preparation, and high operation requirements, and achieve the effects of good water solubility and luminescence properties, simple product purification, and simple synthesis process.
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[0035] A kind of benzothiazole derivative, its preparation method comprises the following steps:
[0036] 1) Add 2mmol of 5-bromoisophthalic acid, 4.4mmol of o-aminothiophenol and 15mL of polyphosphoric acid into a 50mL round bottom flask, heat up to 170°C for 36h, cool the reactant to room temperature, and use NaOH aqueous solution adjusted the pH to 9, a large amount of solids were precipitated, vacuum filtration under reduced pressure, recrystallization of the solid obtained by suction filtration with tetrahydrofuran, to obtain
[0037] 2) Add 0.1mmol of 0.12mmol of 4-ethynyl anisole, 0.01mmol of Pb (PPh 3 ) 2 Cl 2 , 0.01mmol of CuI, 2mL of triethylamine and 2mL of tetrahydrofuran were added to the reaction kettle, reflux reaction at 90°C for 24h, the reaction solution was cooled to room temperature, and 2mL of saturated ammonium chloride solution was added to quench the reaction, and dichloromethane and Ammonium chloride solution was used for extraction, the collect...
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