Alkali-free setting accelerator, and preparation method and application thereof
A technology of accelerator and stabilizer, applied in the field of alkali-free accelerator and its preparation, can solve the problems of long setting time, decline of impermeability level, large dosage, etc., and achieve good stability
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Embodiment 1
[0032] Step 1, mixing sodium metaaluminate with water to obtain a sodium metaaluminate solution;
[0033] Step 2, adding aluminum sulfate to the sodium metaaluminate solution in 3 times to obtain solution I; wherein, stirring for 20 minutes after adding aluminum sulfate each time, the amount of adding aluminum sulfate for the first time is 25% by weight of the total amount of aluminum sulfate The amount of adding aluminum sulfate for the second time is 50% by weight of the total amount of aluminum sulfate, and the amount of adding aluminum sulfate for the last time is 25% by weight of the total amount of aluminum sulfate;
[0034] Step 3, adding fluosilicic acid and hydroxymethylcellulose (complexing stabilizer) to solution I in sequence;
[0035] Wherein, based on the total weight of the alkali-free quick-setting agent, the consumption of sodium metaaluminate is 22% by weight, the consumption of aluminum sulfate is 40% by weight, the consumption of fluosilicic acid is 33% by ...
Embodiment 2
[0037] Step 1, mixing sodium metaaluminate with water to obtain a sodium metaaluminate solution;
[0038] Step 2. Add aluminum sulfate to the sodium metaaluminate solution in 4 times to obtain solution I. After adding aluminum sulfate each time, stir for 20 minutes. The amount of aluminum sulfate added for the first time is 10% by weight of the total amount of aluminum sulfate. The amount of adding aluminum sulfate for the second time and the third time is 40% by weight of the total amount of aluminum sulfate, and the amount of adding aluminum sulfate for the last time is 10% by weight of the total amount of aluminum sulfate;
[0039] Step 3, adding fluosilicic acid and hydroxymethylcellulose to solution I in sequence;
[0040] Wherein, based on the total weight of the alkali-free quick-setting agent, the consumption of sodium metaaluminate is 22% by weight, the consumption of aluminum sulfate is 40% by weight, the consumption of fluosilicic acid is 33% by weight, and the cons...
Embodiment 3
[0042] Step 1, mixing sodium metaaluminate with water to obtain a sodium metaaluminate solution;
[0043] Step 2, adding aluminum sulfate to the sodium metaaluminate solution in 5 times to obtain solution I; wherein, stirring for 20 minutes after adding aluminum sulfate each time, the amount of adding aluminum sulfate for the first time is 10% by weight of the total amount of aluminum sulfate , the amount of adding aluminum sulfate for the second time is 30% by weight of the total amount of aluminum sulfate, the amount of adding aluminum sulfate for the third time is 30% by weight of the total amount of aluminum sulfate, the amount of adding aluminum sulfate for the fourth time is all sulfuric acid 20% by weight of the total amount of aluminum, the amount of adding aluminum sulfate for the last time is 10% by weight of the total amount of aluminum sulfate;
[0044] Step 3, adding fluosilicic acid and hydroxymethylcellulose to solution I in sequence;
[0045] Wherein, based on...
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