Alkali-free setting accelerator, and preparation method and application thereof

A technology of accelerator and stabilizer, applied in the field of alkali-free accelerator and its preparation, can solve the problems of long setting time, decline of impermeability level, large dosage, etc., and achieve good stability

Pending Publication Date: 2020-09-15
SHANXI SUNWAY INTION TRADE CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Alkaline quick-setting agents generally have high alkali content, strong corrosion and easy to cause physical harm to construction workers, and strong alkali characteristics can easily cause alkali-aggregate reaction, which will significantly reduce the later strength of concrete, reduce the impermeability level, and affect the strength of concrete. Durability, not conducive to the construction of the project
However, the existing alkali-free accelerators mainly have the problems of large dosage, long setting time, high viscosity and easy gel aggregation and thickening, and the later strength cannot meet the requirements of engineering construction.

Method used

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  • Alkali-free setting accelerator, and preparation method and application thereof
  • Alkali-free setting accelerator, and preparation method and application thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0032] Step 1, mixing sodium metaaluminate with water to obtain a sodium metaaluminate solution;

[0033] Step 2, adding aluminum sulfate to the sodium metaaluminate solution in 3 times to obtain solution I; wherein, stirring for 20 minutes after adding aluminum sulfate each time, the amount of adding aluminum sulfate for the first time is 25% by weight of the total amount of aluminum sulfate The amount of adding aluminum sulfate for the second time is 50% by weight of the total amount of aluminum sulfate, and the amount of adding aluminum sulfate for the last time is 25% by weight of the total amount of aluminum sulfate;

[0034] Step 3, adding fluosilicic acid and hydroxymethylcellulose (complexing stabilizer) to solution I in sequence;

[0035] Wherein, based on the total weight of the alkali-free quick-setting agent, the consumption of sodium metaaluminate is 22% by weight, the consumption of aluminum sulfate is 40% by weight, the consumption of fluosilicic acid is 33% by ...

Embodiment 2

[0037] Step 1, mixing sodium metaaluminate with water to obtain a sodium metaaluminate solution;

[0038] Step 2. Add aluminum sulfate to the sodium metaaluminate solution in 4 times to obtain solution I. After adding aluminum sulfate each time, stir for 20 minutes. The amount of aluminum sulfate added for the first time is 10% by weight of the total amount of aluminum sulfate. The amount of adding aluminum sulfate for the second time and the third time is 40% by weight of the total amount of aluminum sulfate, and the amount of adding aluminum sulfate for the last time is 10% by weight of the total amount of aluminum sulfate;

[0039] Step 3, adding fluosilicic acid and hydroxymethylcellulose to solution I in sequence;

[0040] Wherein, based on the total weight of the alkali-free quick-setting agent, the consumption of sodium metaaluminate is 22% by weight, the consumption of aluminum sulfate is 40% by weight, the consumption of fluosilicic acid is 33% by weight, and the cons...

Embodiment 3

[0042] Step 1, mixing sodium metaaluminate with water to obtain a sodium metaaluminate solution;

[0043] Step 2, adding aluminum sulfate to the sodium metaaluminate solution in 5 times to obtain solution I; wherein, stirring for 20 minutes after adding aluminum sulfate each time, the amount of adding aluminum sulfate for the first time is 10% by weight of the total amount of aluminum sulfate , the amount of adding aluminum sulfate for the second time is 30% by weight of the total amount of aluminum sulfate, the amount of adding aluminum sulfate for the third time is 30% by weight of the total amount of aluminum sulfate, the amount of adding aluminum sulfate for the fourth time is all sulfuric acid 20% by weight of the total amount of aluminum, the amount of adding aluminum sulfate for the last time is 10% by weight of the total amount of aluminum sulfate;

[0044] Step 3, adding fluosilicic acid and hydroxymethylcellulose to solution I in sequence;

[0045] Wherein, based on...

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Abstract

The invention discloses an alkali-free setting accelerator and a preparation method thereof. The alkali-free setting accelerator is prepared from sodium metaaluminate, aluminum sulfate, fluosilicic acid, a complexing stabilizer and water. The preparation method comprises the following steps: 1, mixing sodium metaaluminate with water to obtain a sodium metaaluminate solution; 2, adding aluminum sulfate into the sodium metaaluminate solution for multiple times to obtain a solution I; and 3, sequentially adding the fluosilicic acid and the complexing stabilizer into the solution I. The alkali-free setting accelerator disclosed by the invention has the advantages of high cement setting and hardening speed, capability of meeting engineering construction requirements in later strength and the like under the condition of low mixing amount.

Description

technical field [0001] The invention relates to an alkali-free accelerator and its preparation method and application. Background technique [0002] Accelerator, as a concrete additive, can effectively shorten the setting and hardening time of cement. Accelerator has a great influence on the setting time and early strength of shotcrete. At present, there are many kinds of accelerators in the market, and they are different. Alkaline quick-setting agents generally have high alkali content, strong corrosion and easy to cause physical harm to construction workers, and strong alkali characteristics can easily cause alkali-aggregate reaction, which will significantly reduce the later strength of concrete, reduce the impermeability level, and affect the strength of concrete. Durability is not conducive to the construction of the project. However, the existing alkali-free accelerators mainly have the problems of large dosage, long setting time, high viscosity, easy to produce gel a...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B24/38C04B28/04C04B103/12
CPCC04B28/04C04B40/0039C04B2103/12C04B22/08C04B22/148C04B22/126C04B24/383C04B14/06
Inventor 李连震王宏维王英维
Owner SHANXI SUNWAY INTION TRADE CO LTD
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