Parathyroid hormone medicine coposition
A parathyroid hormone, hormone technology, applied in the direction of drug combination, drug delivery, pharmaceutical formulation, etc., can solve problems such as large variability
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[0031] Liquid PTH formulations were first prepared prior to lyophilization by mixing human PTH (1-84) as hormone, mannitol as excipient and citrate as buffer.
[0032] The first step of production preparation is to be made into two kinds of mixtures with injectable 20% (w / v) sterile mannitol solution (British Pharmacopeia): add in 20% mannitol solution: (1) lemon acid solution to obtain a mixed solution containing 10mM citric acid and 5% mannitol; (2) sodium citrate monohydrate solution to obtain a second part of a mixed solution containing 10mM citrate and 5% mannitol, the two mixed solutions Miscible in appropriate volume ratios to obtain 5% mannitol solutions with pHs of 4 (±0.2) and 6 (±0.2), respectively.
[0033] Then a certain amount of lyophilized human PTH (1-84) was added to 5% mannitol solution (pH 4 and 6, respectively). PTH is produced by microbial fermentation and needs to be purified and sterilized before freeze-drying. Quantitative PTH was added to the 5% man...
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