Method for digesting free calcium oxide in steelmaking dedusting ash
A technology of free calcium oxide and digestion container, which is applied in the field of solid waste treatment and can solve problems such as potential safety hazards, long time required, iron oxidation, etc.
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Embodiment 1
[0027] The present embodiment provides a kind of digestion method of free calcium oxide in steelmaking dedusting ash, and this digestion method comprises the following steps:
[0028] S1. Put the steelmaking dust removal ash in the digestion container; inject carbon dioxide into the digestion container after vacuuming, and repeat the operations of vacuuming and injecting carbon dioxide until the oxygen content in the gas in the digestion container is <1% v / v;
[0029] S2. Inject saturated water vapor into the digestion vessel and adjust the concentration of carbon dioxide so that the molar weight of water molecules in the saturated water vapor is 65% of the molar weight of carbon dioxide, and the internal pressure of the digestion vessel is kept within the range of 0.18-0.19 MPa;
[0030] S3. Raise the temperature in the digestion vessel to 200°C at a rate of 65°C / min, keep it at 190-210°C for 20 minutes, and use a pre-cooled to 7°C under the condition that the pressure in the ...
Embodiment 2
[0032] The present embodiment provides a kind of digestion method of free calcium oxide in steelmaking dedusting ash, and this digestion method comprises the following steps:
[0033] S1. Put the steelmaking dust removal ash in the digestion container; inject carbon dioxide into the digestion container after vacuuming, and repeat the operations of vacuuming and injecting carbon dioxide until the oxygen content in the gas in the digestion container is <1% v / v;
[0034] S2. Inject saturated water vapor into the digestion vessel and adjust the concentration of carbon dioxide so that the molar weight of water molecules in the saturated water vapor is 50% of the molar weight of carbon dioxide, and the internal pressure of the digestion vessel is kept within the range of 0.16-0.18 MPa;
[0035] S3. Raise the temperature in the digestion vessel to 240°C at a rate of 80°C / min, keep it at 230-250°C for 15 minutes, and use a pre-cooled to 5°C under the condition that the pressure in the ...
Embodiment 3
[0037] The present embodiment provides a kind of digestion method of free calcium oxide in steelmaking dedusting ash, and this digestion method comprises the following steps:
[0038] S1. Put the steelmaking dust removal ash in the digestion container; inject carbon dioxide into the digestion container after vacuuming, and repeat the operations of vacuuming and injecting carbon dioxide until the oxygen content in the gas in the digestion container is <1% v / v;
[0039] S2. Inject saturated water vapor into the digestion vessel and adjust the concentration of carbon dioxide so that the molar weight of water molecules in the saturated water vapor is 80% of the molar weight of carbon dioxide, and the internal pressure of the digestion vessel is kept within the range of 0.18-0.20 MPa;
[0040]S3. Raise the temperature in the digestion vessel to 160°C at a rate of 50°C / min, and keep it at 150-170°C for 30 minutes. Carbon dioxide replaces the gas in the digestion vessel, and cools th...
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