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A kind of polycrystalline diamond composite sheet and preparation method thereof

A technology of polycrystalline diamond and composite sheet, which is applied in metal material coating process, vacuum evaporation plating, coating, etc., can solve the problem that polycrystalline diamond composite sheet cannot have both high wear resistance and heat resistance, etc. Achieve the effects of improving thermal conductivity, excellent mechanical and thermal properties, and benefiting residual stress

Active Publication Date: 2022-06-07
ZHONGNAN DIAMOND CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0004] In order to overcome the problems in the prior art, the present invention provides a polycrystalline diamond composite sheet with good heat resistance and its preparation method, which solves the problem that the polycrystalline diamond composite sheet cannot have both high wear resistance and heat resistance

Method used

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  • A kind of polycrystalline diamond composite sheet and preparation method thereof
  • A kind of polycrystalline diamond composite sheet and preparation method thereof
  • A kind of polycrystalline diamond composite sheet and preparation method thereof

Examples

Experimental program
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Effect test

Embodiment 1

[0040] The polycrystalline diamond compact sheet with good heat resistance in this embodiment includes a cemented carbide substrate, a transition coating and a polycrystalline diamond layer sequentially arranged on the cemented carbide substrate; the polycrystalline diamond layer is composed of the following weight percentages Composition of raw materials: 69.5% of coated diamond powder, 20% of coated cubic boron nitride powder, 0.3% of carbon nanotubes, 0.2% of graphene and 10% of binder; the transition coating is Si in order 3 N 4 coating and Si coating, the Si 3 N 4 The thickness of the coating is 10 μm, and the thickness of the Si coating is 15 μm; the coating of the coated diamond micro-powder is Si, and the thickness of the coating is 80 nm, and the coated diamond micro-powder is boron-containing diamond micro-powder, and boron element in the boron-containing diamond micro-powder The content is 0.0002 to 1%; the coating of the coated cubic boron nitride micro-powder is...

Embodiment 2

[0054] The polycrystalline diamond compact sheet with good heat resistance of this embodiment includes a cemented carbide base, a transition coating and a polycrystalline diamond layer sequentially arranged on the cemented carbide base; the polycrystalline diamond layer is composed of the following weight percentages Raw material composition: 79.7% of coated diamond powder, 15% of coated cubic boron nitride powder, 0.2% of carbon nanotube, 0.1% of graphene and 5% of binder; the transition coating is Si in order 3 N 4 Coatings and Si coatings, Si 3 N 4 The thickness of the coating is 6 μm, and the thickness of the Si coating is 10 μm; the coating of the coated diamond micro-powder is W, and the thickness of the coating is 120 nm; the coated diamond micro-powder is a boron-containing diamond micro-powder, and the boron element of the boron-containing diamond micro-powder is The content is 0.0002 to 1%; the coating of the coated cubic boron nitride micro-powder is Ti, and the t...

Embodiment 3

[0067] The polycrystalline diamond compact sheet with good heat resistance of this embodiment includes a cemented carbide base, a transition coating and a polycrystalline diamond layer sequentially arranged on the cemented carbide base; the polycrystalline diamond layer is composed of the following weight percentages Composition of raw materials: 74.6% of coated diamond powder, 17.5% of coated cubic boron nitride powder, 0.25% of carbon nanotubes, 0.15% of graphene and 7.5% of binder; the transition coating is Si in order 3 N 4 Coatings and Si coatings, Si 3 N 4 The thickness of the coating is 8 μm, and the thickness of the Si coating is 12.5 μm; the coating of the coated diamond micro-powder is Ni, and the thickness of the coating is 100 nm; the coated diamond micro-powder is a boron-containing diamond The element content is 0.0002-1%; the coating layer of the coated cubic boron nitride micro-powder is Mo, and the coating thickness is 100 nm; the particle size of the coated...

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Abstract

The invention belongs to the technical field of superhard materials, and in particular relates to a polycrystalline diamond composite sheet with good heat resistance and a preparation method thereof. The polycrystalline diamond composite sheet includes a cemented carbide substrate and a transition coating and a polycrystalline diamond layer successively arranged on the cemented carbide substrate; the transition coating is successively Si 3 N 4 coating and Si coating; the polycrystalline diamond layer includes the following raw materials in weight percentage: 69.5-79.7% of coated diamond powder, 15-20% of coated cubic boron nitride powder, 0.2-0.3% of carbon nanotube, graphite Alkenes 0.1-0.2% and binders 5-10%. The present invention adopts coated diamond micropowder and cubic boron nitride micropowder, adds carbon nanotubes and graphene materials in the polycrystalline diamond layer, and breaks through the technical bottleneck of high toughness, high heat resistance and high wear resistance of polycrystalline diamond composite sheet , the prepared polycrystalline diamond compact has excellent heat resistance and wear resistance compared with the diamond compact obtained in the prior art.

Description

technical field [0001] The invention belongs to the technical field of superhard materials, in particular to a polycrystalline diamond composite sheet with good heat resistance and a preparation method thereof. Background technique [0002] The polycrystalline diamond composite sheet is made of cemented carbide as the matrix, supplemented by a layer of diamond powder mixed with different binders and sintered at high temperature and high pressure. Because it has the characteristics of high diamond hardness and good wear resistance, it is also It has the characteristics of strong impact resistance and good weldability of cemented carbide, so it is widely used in the field of cutting of non-ferrous metals and difficult-to-machine non-metallic materials. [0003] In the prior art, the common polycrystalline diamond composite sheet is sintered from diamond-cobalt series. During the high pressure and high temperature sintering process of the polycrystalline diamond composite sheet...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B22F7/04B22F3/14B22F3/24C22C26/00C23C14/06C23C14/16C23C14/35
CPCB22F7/04B22F3/14B22F3/24C23C14/0652C23C14/165C23C14/0036C23C14/35C22C26/00B22F2007/042B22F2003/248C22C2026/002C22C2026/007B22F2998/10
Inventor 张涛卢灿华朱培宋子衡昝亚男
Owner ZHONGNAN DIAMOND CO LTD