Fragrance-carrying supramolecular gel based on gallic acid nicotine salt gelling agent
A technology of supramolecular gel and gallic acid, which is applied in the field of fragrance-carrying supramolecular gel, can solve the problems of mutual repulsion, volatilization loss of fragrance components, and failure to bring characteristic fragrance, so as to reduce raw material and manufacturing costs, and reduce smoke volume Small, to avoid the effect of too fast loss
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Embodiment 1
[0077] A preparation method of fragrance-loaded supramolecular gel based on nicotine gallic acid salt gelling agent, comprising the steps of:
[0078] Step 1, preparation of the gelling agent: the gallic acid and nicotine are respectively dissolved in a mixed solvent of water and ethanol in a molar ratio of 2:1, and the mass volume ratio of the mixed solvent of gallic acid and the water and ethanol dissolved therein is 1g:28mL The mass volume ratio of nicotine to the water and ethanol that dissolves it is 1g:210mL, and it is stirred at room temperature until it is completely dissolved to obtain gallic acid solution and nicotine solution respectively, and then the above two solutions are fully mixed to obtain a mixed solution, The mixed solution was heated to reflux, reacted for more than 30 minutes, 170 mbar, 53 ° C rotary evaporation, and then the product obtained by the rotary evaporation was dried at 36 ° C for 24 hours to obtain nicotine gallate salt gelling agent. In the ...
Embodiment 2
[0084] This example provides the application of the fragrance-loaded supramolecular gel prepared in Example 1 of the present invention in heating cigarettes
[0085] The nicotine salt supramolecular gel can be respectively applied in the manufacturing process of the reconstituted tobacco leaf for paper-making heated cigarettes and the reconstituted tobacco leaf for heated cigarettes heated by thick pulp method, and can be applied as a single gel or mixed gels of different types according to actual conditions.
[0086] Reconstituted tobacco leaves for paper-making heated cigarettes:
[0087] Method 1: Add the fragrance-carrying supramolecular gel prepared in Example 1 to a certain amount of fuming agent (1,2-propanediol, glycerin or a mixture of the two in a certain proportion), the quality of the fragrance-carrying supramolecular gel and the fuming agent The ratio is 5:1, the temperature is raised to 90°C, the gel melts into a sol state or a solution, and is uniformly mixed to...
Embodiment 3
[0099] This example provides the application of the fragrance-loaded supramolecular gel prepared in Example 1 in electronic cigarettes.
[0100] The nicotine salt supramolecular gel can be applied in electronic cigarettes in two ways, and a single gel or different types of mixed gels can be used according to actual conditions.
[0101] Method 1: Dry the fragrance-carrying supramolecular gel prepared in Example 1 above at a constant temperature in an oven at 40°C for 24-36 hours, grind the dried gel into uniform micro-particles, and add a certain amount of e-cigarette gel in a certain proportion. Fully stir in the fuming agent, the fuming agent is a mixed solvent of glycerin and 1,2-propanediol 1.2:1 (volume ratio), the mass ratio of the fragrance-carrying supramolecular gel to the fuming agent is 1:120, mix well and serve as The flavor-containing gel smoking agent or as an auxiliary material is directly added to the finished e-liquid and mixed uniformly as the flavor-containin...
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