A kind of detection method of cysteine
A cysteine and detection method technology, applied in the cysteine detection field, can solve the problems of expensive instruments and equipment, long detection time and the like, and achieve the effects of simple and convenient preparation method, rapid detection and high sensitivity
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Embodiment 1
[0025] A method for synthesizing C-N@GC nanomaterials, comprising the following steps:
[0026] (1) Synthesis of ZIF-8: Pour the methanol solution of 2-methylimidazole (6.16 g, 150 mL) into Zn(NO) 2 ·6H 2 O in methanol solution (5.95g, 150mL); secondly, the above-mentioned mixed solution was stirred at room temperature for 24h to obtain a milky white liquid; then the milky white liquid was washed 3 times with methanol and collected by centrifuge; finally, under the condition of 60 degrees Celsius Dry in vacuo overnight to give ZIF-8; and 2-methylimidazole with Zn(NO) 2 ·6H 2 The mass ratio of O is 6.16:5.95;
[0027] (2) Synthesis of ZIF-8@ZIF-67: The ZIF-8 (0.5 g) synthesized in step (1) was dispersed in methanol solution (100 mL) with ultrasonic waves, and after stirring for 10 min, 2-methylimidazole in methanol Solution (6.16g, 100mL) and Co(NO) 2 ·6H 2 The methanol solution of O (5.82g, 100mL) was poured into the above solution; secondly, the mixed solution was stirr...
Embodiment 2
[0030] The application of C-N@GC nanomaterials in cysteine detection includes the following steps:
[0031] S1, configuration of modifier solution: take 5 mg of C-N@GC synthesized in Example 1 and transfer it to a mortar, fully grind it into powder, and put the ground C-N@GC into 1 ml of water-ethanol solution ( volume ratio 3:1), so that the ground C-N@GC can be uniformly dispersed in 1 ml of water-ethanol solution (volume ratio 3:1), and 20 μL of naphthol solution (5wt%) was added dropwise to it, A uniform modifier solution was obtained by ultrasonication for 2 h by ultrasonic degradation;
[0032] S2. Modification on the surface of the glassy carbon electrode: take 3 μL of the modifier solution in S1 and drop it evenly on the surface of the polished glassy carbon electrode, and dry it at room temperature to finally obtain a C-N@GC modified glassy carbon electrode;
[0033] S3. The C-N@GC modified glassy carbon electrode obtained in S2 is used for the electrochemical dete...
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