Water body pollution repairing agent and preparation method thereof
A water pollution and restoration agent technology, applied in the field of water pollution control, can solve problems such as secondary pollution, adsorbents that cannot be reused, and insufficient adsorption capacity
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Embodiment 1
[0030] A water body pollution remediation agent, by weight parts, mainly includes:
[0031] 10 parts of modified chitosan fiber, 2 parts of modified graphene oxide.
[0032] A kind of preparation method of water body pollution remediation agent, the preparation method of described water body pollution remediation agent is:
[0033] (1) Immerse graphene oxide in an ammonium azide solution 5 times the mass of graphene oxide, sonicate at 40kHz, 200W and heat to 100°C, react until no gas escapes, centrifuge and wash with absolute ethanol 3 times, dried to constant weight, prepared pre-modified graphene oxide;
[0034] (2) Disperse disodium edetate in deionized water with 5 times the mass of disodium edetate to obtain a disodium edetate dispersion, and mix the pre-modified graphene oxide suspension with The disodium edetate dispersion was mixed at a mass ratio of 2:1, ultrasonicated at 40kHz and 200W for 2h, transferred to a drying oven, dried at 60°C to constant weight, washed 3...
Embodiment 2
[0044] A water body pollution remediation agent, by weight parts, mainly includes:
[0045] 10 parts of modified chitosan fiber, 2 parts of modified graphene oxide.
[0046] A kind of preparation method of water body pollution remediation agent, the preparation method of described water body pollution remediation agent is:
[0047] (1) Immerse graphene oxide in an ammonium azide solution 10 times the mass of graphene oxide, sonicate at 40kHz and 200W and heat to 120°C. After reacting until no gas escapes, centrifuge and wash with absolute ethanol 5 times, dried to constant weight, prepared pre-modified graphene oxide;
[0048] (2) Disperse disodium edetate in deionized water with 10 times the mass of disodium edetate to obtain a disodium edetate dispersion, and mix the pre-modified graphene oxide suspension with The disodium edetate dispersion was mixed at a mass ratio of 2:1, ultrasonicated at 40kHz and 200W for 2h, transferred to a drying oven, dried at 60°C to constant we...
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