Preparation method of rare earth composite material
A composite material and rare earth technology, applied in the field of metal materials, can solve the problems of insufficient mechanical properties, difficult structural parts, poor energy release effect, etc., and achieve the effect of good energy release effect.
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Embodiment 1
[0043] The preparation method of the rare earth composite material of the present embodiment includes the following steps:
[0044] Raw material mixing: M powder with a particle size D50 of 6.0 μm and 58# paraffin are put into the mixer according to the ratio of 99:1 to 98:2 for mixing, and the mixing time is 24h.
[0045] Compression molding: put the mixed powder into a rubber sleeve, and press and shape in an isostatic press according to the compression pressures of Examples 1.1-1.8 and Comparative Examples 1.1-1.2 in Table 1, and hold the pressure for 30s.
[0046] Degreasing: Place the formed body in trichloroethylene solvent at 50°C to remove part of the 58# paraffin, and then perform thermal degreasing at 500°C.
[0047] Sintering treatment: put the compact into a vacuum furnace, fill the furnace with hydrogen and heat it up to 2100°C, sinter for 10 hours, and obtain M skeleton after cooling in the furnace.
[0048] Infiltration treatment: put the rare earth element int...
Embodiment 2
[0065] The preparation method of the rare earth and tungsten composite material of the present embodiment includes the following steps:
[0066] Raw material configuration and mixing: Put tungsten powder with a particle size D50 of 7.0μm and 58# paraffin into the mixer according to the ratio of 99:1 to 98:2, and the mixing time is 36h.
[0067] Compression molding: Put the mixed powder into a rubber sleeve, and press and shape in an isostatic press according to the compression pressures of Examples 2.1-2.8 and Comparative Examples 2.1-2.2 in Table 4, and the pressure holding time is 25s.
[0068] Degreasing: Place the formed body in trichloroethylene solvent at 70°C to remove part of the 58# paraffin, and then perform thermal degreasing at 450°C.
[0069] Sintering and dehydrogenation: put the compact into a vacuum furnace, fill the furnace with hydrogen and heat it up to 2100 ° C, sinter for 10 hours, and obtain a tungsten skeleton after cooling in the furnace.
[0070] Infi...
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