Technique for extracting rose essential oil

A technology of rose essential oil and extraction method, which is applied in the direction of essential oil/fragrance, fat production, etc. It can solve the problems affecting the yield and purity of rose oil, the incomplete separation of oil and water, and the quality of rose oil, and achieves easy cleaning and heating The effect of fast speed and easy cleaning

Inactive Publication Date: 2005-12-21
ZHEJIANG KAIDI PHARMA CHEM MACHINERY
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Problems solved by technology

Since this extraction method uses a conical retort up and down, and uses dry steam to directly pass into the retort for heating, the residue after distillation can only be dug out manually in the hole on the side of the retort, and the roses are attached to the retort. Due to the coking phenomenon caused by high temperature on the pipe, it is very difficult to clean, and it is very labor-intensive and time-consuming. Since the dry steam is used without separation and purification, the heat source and impurities in the steam directly damage the roses during the entire static thermal reaction process. Composition and properties make the distilled rose oil turbid and smelly, black spots remain in the oil, which affects the quality of rose oil, and this method uses a tubular condenser for cooling, so that the rose oil The gas and liquid cannot be completely cooled when entering the condenser, resulting in the loss of rose oil gas and liquid. At the same time, an oil-water separator is used for separation, so that the oil and water cannot be completely separated, which directly affects the yield and purity of rose oil.

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  • Technique for extracting rose essential oil

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[0007] The accompanying drawings show the implementation process of the method of the present invention, and further describe the relevant details of its embodiments below in conjunction with the accompanying drawings. The extraction method of the rose essential oil is firstly to mix roses and water into a pneumatic open and close distillation tank, then pass steam into the jacket of the pneumatic open and close distillation tank, and use a stirring device to distill in the pneumatic open and close The tank is heated while stirring, and the steam generated in the pneumatic open-close distillation tank is subjected to secondary distillation of the distillation column, condensed by the condenser, cooled by the cooler, and then subjected to secondary oil-water separation, and finally the rose essential oil product is obtained; During the heating process, the temperature should be controlled at 100-120°C; the water after secondary separation flows back into the distillation tank an...

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Abstract

The invention discloses a method for extracting rose essential oil, which is characterized by mixing roses and water into a pneumatic opening and closing retort, then passing steam into the jacket of the pneumatic opening and closing retort, and using a stirring device Heating while stirring is carried out in the pneumatic open and closed distillation tank. After the steam generated in the pneumatic open and closed distillation tank is subjected to the secondary distillation of the distillation column, it is condensed by the condenser and cooled by the cooler, and then the secondary oil and water are separated. Get rose essential oil products. In the present invention, steam is introduced into the jacket of the distillation tank for heating. Due to the large heating area and fast heating speed, after the roses and water in the distillation tank are heated, the thermal reaction is carried out in a dynamic state under the stirring of the stirring device. , without affecting the internal quality of roses, maintaining the original properties and transparency of roses, using secondary oil-water separation, the oil and water are completely separated, and the quality, yield and purity of rose essential oil are improved.

Description

【Technical field】 [0001] The invention relates to a method for extracting Chinese medicinal materials, in particular to a method for extracting rose essential oil. 【Background technique】 [0002] In the prior art, the extraction method of rose essential oil is to put roses and water into the upper and lower conical distillation tanks to directly heat the water, and the heated steam is condensed through the tubular condenser, and then passed through the oil-water separator Separation to obtain rose essential oil. Since this extraction method uses a conical retort up and down, and uses dry steam to directly pass into the retort for heating, the residue after distillation can only be dug out manually in the hole on the side of the retort, and the roses are attached to the retort. Due to the coking phenomenon caused by high temperature on the pipe, it is very difficult to clean, and it is very labor-intensive and time-consuming. Since the dry steam is use...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C11B9/00
Inventor 邱云彪高延厅胡秀麟
Owner ZHEJIANG KAIDI PHARMA CHEM MACHINERY
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